GCMS calibration table for PCBs and PAHs, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0901\LBB.D Vial: 16 Acq On : 10 Nov 2001 3:02 am Operator: 209 GALOS Sample : lb blk 10/23 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M {RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.89 ug/1 317885 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hwroxy-4-methyl- 116 C6H12O2 000123-42-2 72 2 Acetic acid, 1, dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Acetone 58 C3H6O 000067-64-1 10 4 3-Hydroxy-2-p^•tanone 102 C5H10O2 003142-66-3 9 Mjundance / Scan 289 (7.694 min): LBB.D (-) m/z43.00 100.00%

5000 59

101 .. iJ 77;--- '7.40' lS' 7.^ 8.00' ' 53,. 83 ........ • I • • • ■ I ‘ ‘^< ,l| 1 I ' I ' ■■'■I I ' r-f-r-r-r-r-] —rh- I I • • • I I I ■ • • I ‘ m/z 59.05 49.10% nfz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- <113

5000 59 7.40 7.60 7.80 8.00 m/z 101.05 2^793% 27 101 ........................ II TiZz-> ' 'ib'' "2b“ “S’ ' I ’ ‘ ‘ 1 * ’ ‘ ' I ' 40 50 60 70 80 90 100 110 Abundance #3292: Acetic add, 1,1 -dimethylethyl ester

' 7.^ 7.S 7.S abb ' 5000 57 m/z 58.05 18.16% 101 15 27 Ti&-> 10^20^30 '40' ' ' '50' ' ' 1 ‘ ' I ' ' ' ' I ' ' ' ' I ‘ ‘ ‘ I ' ' ' ' I ' 60 70 80 90 100 110 Abundance #62326: Acetone 4(3 •7.^ 'n*" 7.60 7.80 8.00 m/z 41.00 7.85% 5000- 58

nfe-> 10 20 30 40 50 60 70 80 90 100 110 tIotStJosSo

LBB.D NP103001.M Wed Nov 28 14:48:36 2001 Page 1

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