Calibration data table for TCLP analysis including retention times and response factors for various compounds.
NYC-WTC_000086981–000087006Folder label: “508 Scan 9/17/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample 9/17 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table- 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T. 7.77 0.99 ug/1 132999 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual
1 2-Pen^none, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Propme, 1-ethoxy-2-methyl- 102 C6H14O 000627-02-1 17 3 3-H^roxy-3-methyl-2-butanone 4 5-Hexen-2-one Abundance Scan 297 (7.768 min): LBD.D (-) 4)3 102 98 C5H10O2 C6H10O 5=^ 000115-22-0 17 000109-49-9 9
59 5000
101 7.40 7.60 7.80 8.00 8.20 53 , I ' ' ' I ' '9'1 I 69 83 i I ' ' ' ' I ' I ' ' ' ' I ' ' ' ' I Tife-> <\bundance 10 20 30 40 50 60 70 #64275: 2-Pentanone, 4-hydroxy-4-methyl- 40 80 90 100 110 ..... ’; 5000 59 7.40 7.60 7.80 8.00 8.20 m/z 101.05 21.27% 15 31 101 I I 83 '1^ n-*- ....... 'I Hy-r-r-i-T-j-r-r-r-T-p-r^ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1772: Propane, 1-ethoxy-2-methyl- 31 50 7 40 7.60 7.80 8.00 8.20 5000 m/z 58.05 16.54%
I . Il I I 45 . I I 4 ' I ' ' ' ' I 73 '' I . . I ■ 102 ' I ' ' I I I I ' I I I
nz •n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1697: 3-Hydroxy-3-methyl-2-butanone I 5)9 7.40 7.60 7.80 8.00 8.20
5000 43 31
39... 69................87............................ I ' ‘ ' I ' ' ' ' I ' I ' ' ''' I I Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00 8.20
LBD.D NP091101.M Tue Oct 02 12:28:20 2001 Page 5
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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