GCMS blank results, sample AD31129, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0802\LBD.D Vial: 17 Acq On : 10 Jan 2002 5:25 am Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.59 1.23 ug/1 332492 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, A-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 83 2 Acetic acid,/1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 CH2=CHCH2C(®)OCH3 100 C5H802 003724-55-8 10 4 3 -Hydroxy-2 -pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 277 (7.590 mln): LBD.D (-) m/z 42.95 100.00% 43

5000 59

101 f • » » i । "I i » I । PTTPTTTIT 7.20 7.40 7.60 7.80 8,00

m/z-> ................... 37, . 10 20 30 40 +50+ 50 69 83 1 ’ I•‘‘ ‘ I ’ *' ‘11 60 70 80 90 1 i 1 1 1 ■ i 100 110 m/z 59.05 44.76% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43 -______ /... 5000 59 7.20 7.40 7.60 7.80 8.00 m/z 101.05 17.39% 27 101

m/z-> 10 20 30 40 + +4950—+ I60umpmTm 70 80 83 90 - 100 110 Abundance Asott 3C i. 1 drefv.t 43 1111111 TTnt 7.20 7.40 7.60 7.80 8.00 5000 57 m/ z 58.0,5 16.14% 101 15 27 ■ ■ i ■ ■ ■ ■ I ■ ■ ■ ■ I 1 1 1 1 I ri • ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ i • • ■ • i ■ ■ ■ ' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 T 43 7.20 7.40 7.60 7.80 8.00 m/z 41.05 6.08% 5000

... . 381 58 72 100 ■ 1 i ‘ • i ‘ 1 ■ ■ t ■ ■ ■ • I* T1*mmurfpfrrm m/z~> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

LBD.D GCMS0103.M Wed Feb 06 09:20:15 2002 Page 2

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