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GCMS analysis results for sample AE10900, May 21 2002

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Laboratory report detailing GCMS analysis of sample AE10900 conducted on May 21, 2002, including surrogate recovery data.

NYC-WTC_000024141–000024152

Folder label: “GCMS X 5/10/02 A 5/16/02

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NYC 9/11 Public Portal Document Llorary searcr compound Keport

Data File : C:\MSDCHEM\l\DATA\051602\10900.D Vial: 13 Acq On : 17 May 2002 12:19 am Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 Anthracene, 2-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.28 ug/L 306565 Phenanthranene- dl 0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59* 3 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H130P 1000196-97-5 59 4 Anthracene, 1-methyl- 192 C15H12 000610-48-0 53 Abundance Scan 3319 (22.580 min): 10900.D (-3312) (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.20 22.40 22.60 22.80 23.00

mfe-> 0 42 70 |, , 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 120 I I m/ z 191.00 25.35% Abundance #125845: Anthracene, 2-methyl- 192

5000 TI 1‘‘‘I 22.20 22.40 22.60 22.80 23.00 m/z 193.10 15.38% 96 165 . 66 75 87 | 115 126 139 152 | 176 0 11" " i11111"111" ‘1111" i' I’li i'1'1 ''''i ■ rr1 ‘1111''' i ■ ■1 ■ i ■ ■ "'i ■" ■ r1 ■" ।111 ■ ।' 'i'11'1 ‘t T1p m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 192 1 1 1 1 ’ ' 1 ‘ * ■ • i ■ ■ 11 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 14.66%

28 39 51 63 82 96 115 126 139 152 165 176 o! ■ i' ■ 1"' ■ I1" ■11. ...... . r1'1 "‘ll'111,111 ■" i 11'" ■ i'' '•■‘i'T1'111 tt ‘ r- rtr1 r TTT miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- A 192 22.20 22.40 22.60 22.80 23.00 164 rn/z 160,10 12.78%

5000 99 115 47 77 177 67 125 146

mfz-> 0 — 27.39. +4457,4 . .. . 87. HTT 134,41,155, HH TTTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 _----- 22.20 22.40 22.60 22.80 23.00

10900.D 050102.M Fri May 17 15:08:16 2002 Page 6

NYC-WTC_000024150

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NYC-WTC_000024150Source: NYC Law Department, mirrored locally

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