GCMS sample AE11905 results, June 6 2002

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Gas chromatography-mass spectrometry analysis report for sample AE11905 detecting unknown compounds and surrogates on June 6, 2002.

NYC-WTC_000015581–000015605

Folder label: “GCMS X 6/4/02 A 6/4/02”

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NYC 9/11 Public Portal Document Llbrary searcn compound Keport

Data File C:\MSDCHEM\l\DATA\060402\11905.D Vial: 8 Acq On 4 Jun 2002 9:33 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 15 Anthracene, 2-methyl- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.25 ug/L 252163 Phenant hr anene - d 10 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 45 2 lH-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 42 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 40 Abundance Scan 3311 (22.533 min): 11905.D (-3301) (-) m/z 192.10 100.00% 192

5000

146 1 22.20 22.40 22.60 22.80 ' ' 118 0 TIWTWWTIWTWPWTTTWTUI"TTTTTPTTTT mHTTTT-- 70 82 T 160 +rp m/z 193.00 18.32% m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140 150160170180190 200 Abundance #81034: Anthracene, 2-methyl- 192

5000 22.20 22.40 22.60 22.80 m/z 146.10 18.25% 82 96 165 18 27 39 51 69 | || 115 126 139 152 | 176 , 0- TTTTTTTTTTTTTTTTTTTTNTTTTTTTNTTTTTTTTTHTTHTT TTr miz-> 10 20 30 40 50 60 70 80 90 100110120130140 150160170180190200 Abundance #80945:1H-2-lndenone,2,4,5,6,7,7a-hexahydro-3-(1-methylet... 192 A 1 149 22.20 22.40 22.60 22.80 177 5000 m/z 191.00 17.75% 41 93 107 121 135 164 55 67 79 27

miz-> Ot mHHH,#44 al++ le 14 A 1 A# Imopal . TTH TTTI 10 20 30 40 50 60 70 80 90 100110120130140 150160170180190200 HAirmro, M Abundance #80953:2-PropenaI, 3-(3,4-dimethoxypheny!)- 192 22.20 22.40 22.60 22.80 ‘ ‘ ‘ 161 m/z 96.10 11.88% 5000 77 121 149 91 103 52 64 138 0- t> 11 itrp i > i! i > > • । ■ 111 J1!1, >. । jl 111, i, .... I i i" ■ ■ i ■ TI’T T-r-p-i-r-r-p-r i ' 1 1 ■ i ■ ' ■ ■ i nfe-> 10 20 30 40 50 60 70 80 90 100110120130140 150160170180190 200 22.20 22.40 22.60 22.80

11905.D 060302.M Wed Jun 05 14:03:56 2002 Page 18

NYC-WTC_000015603

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