GCMS sample AE11905 results, June 6 2002

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Gas chromatography-mass spectrometry analysis report for sample AE11905 detecting unknown compounds and surrogates on June 6, 2002.

NYC-WTC_000015581–000015605

Folder label: “GCMS X 6/4/02 A 6/4/02”

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NYC 9/11 Public Portal Document Library aearen compound Report

Data File C:\MSDCHEM\1\DATA\060402\11905.D Vial: 8 Acq On 4 Jun 2002 9:33 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Anthracene-dlO- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

23.06 0.31 ug/L 309572 Phenant hranerie - dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 93 2 Phenanthrene-diO 188 C14D10 001517-22-2 90 3 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 45 4 3-Amino-4-methyl -6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3401 (23.062 min): 11905.D (-3393) (-) m/z 188.10 100.00% 188

5000 . ............................................. 80 94

m/z-> 0 --HH 36 66 „lil 1101101’1111111111511111111111111311"11117 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 i ■ ■" 22.80 23.00 23.20 23.40 m/z 184.10 16.22% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 80.10 15.80% 80 94 160 , . 17 30 42 52 O 0 'l | 1 1 ■ ■ | I I . I p i! I | I I I . | II I I | I I I ! | I . I I I 1 1 l’| iit .. .................................................................. mlz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 .............................................. 22.80 23.00 23.20 23,40 5000 m/z 189.10 14.95%

94 80 160 30 42 52 11 66 „ 108118 132 146 ,|.I 170179/1 0 11111111"11 ■111111111111111111 rri" i'" I [ H ■ i,»t»11 ■ 1111 n i ■ 11 ■ I ■ 11 ■ I n i i'lT|li ■ 11 p i ■ rTTTt mi mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... 188 22.80 23.00 23.20 23.40 m/z 94.05 13.50%

5000- 79 91 55 67 1nc 131 10 117 iz—> - O1!"! I ■ 11 l I I 11 ] > I > 1 j > 100111—0011—001100011’137/181 145 152173..Il ‘ ‘ ' ■ 1 1-1 1 1 1 r 1 1 ' | 1 1 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11905.D 060302.M Wed Jun 05 14:03:57 2002 Page 19

NYC-WTC_000015604

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