GCMS analysis results for sample AE10899, May 21 2002

NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\l\DATA\051602\10899.D Vial: 12 Acq On : 16 May 2002 11:30 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 3 Dodecane, 3-methyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 23.11 1.17 ug/L 1409330 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dodecane, 3-methyl- 184 C13H28 017312-57-1 70 2 Eicosane 282 C20H42 000112-95-8 58 3 Octacosane 394 C28H58 000630-02-4 58 4 Pentadecane 212 C15H32 000629-62-9 58 Abundance Scan 3410 (23.115 min): 10899.D (-3402) (-) m/ z 57.20 100.00% 57 188

5000 85

— 22.80 23.00 23.20 23.40 0 4441404 TTp-rrTp-rrrp-rTTp-rTTp-rrrp-rrTp-rT^^ m/z 71.10 76.47% mlz-> 20 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 Abundance #112341: Dodecane, 3-methyl- 57

5000 85 22.80 23.00 23.20 2340 ' 155 29 m/ z 43.20 70.73%

miz-> 0 1‘ “11 J T7 184

20 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380 Abundance #112345: Eicosane • 57 CTpREtPPr 22.80 23.00 23.20 23.40 5000 m/z 188.10 68.02% 85 29

miz-> 0 4 111], 141 . 169 197 225 253 282 । 11 ‘11* , "I ‘h41—4ul‘utt /T+dooi‘‘h" 1*7" rq i i i ! |‘i > up u i | i , i i | > Immrn TrTTTr 20 40 60 80 100120140160180 200 220 240 260 280300 320 340 360 380 Abundance #11 2312: Octacosane 57 22.80 23.00 23.20 23.40 m/z 85.10 46.35% 5000 85

iz-> 0 JU Jl 1 1113,141 169 197 225 253 281 309 337 365 394 'I ’T ’T"7 . ,T, | r. . .p..'. | rf.. |'i . 11’|. (r.|> 111 II | I! 11| I u > 11 n 111 20 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380 AAL 22.80 23.00 23.20 23.40

10899.D 050102.M Fri May 17 15:07:28 2002 Page 8

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