GCMS analysis results for sample AE10899, May 21 2002

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Data File : C:\MSDCHEM\l\DATA\051602\10899.D Vial: 12 Acg On : 16 May 2002 11:30 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Phosphonic acid, dioctadecy... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.00 28.78 ug/L 33864900 Chrysene-dl2 ■ 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9(93 2 1-Octadecanol 270 C18H38O 000112-92-5 81 3 10-Heneicosene (c,t) 294 C21H42 095008-11-0 74 4 Cycloeicosane 280 C20H40 000296-56-0 74 Abundance Scan 4412 (29.002 min): 10899.D (-4402) (-) m/ z 55.10 100.00% 55

5000 69 83 97 41 111 127

miz-> 0! 1111 20 40 —l I ll, |, ' 60 + .nl ll 141155169183197211225239252267281295 80 100 120 140 160 180 200 220 240 260 280 300 28.60 28.80 29.00 29.20 29.40 m/z 43.15 51.04% Abundance #13890: Phosphonic acid, dioctadecyl ester 55 69 83 41 97

5000 ................... ) 111 28.60 28.80 29.00 29.20 29.40 136 m/ z 57.15 49.03% 14 2 1 I O’ -l Hlell "111 1111... mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5273:1-Octadecanol ■ 43 57 83 97 ................. )...............- 28.60 28.80 29.00 29.20 29.40 5000 111 m/z 83.05 47.19% 29 125

0 — TT TT miz->20 40 60 80 M„1153168182196209221,252 100 120 140 160 180 200 220 240 260 280 300 Abundance #13500:10-Heneicosene(c,t) I ' ' 1 ' I ' 1 >TT7 4 55 69 83 28.60 28.80 29.00 29.20 29.40 97 m/ z 73.10 41.49% 5000 111 27 125

rn/z—> 0 14,11 20 40 IT 60 k a1 139153167.... F’tl 1। * i IT’ 111 1111111111 I 1 ‘ 11 I 80 100 120 140 160 180 200 220 240 260 280 300 294 I '11 ■ i 11111 ' 28.60 28.80 29.00 29.20 29.40

10899.D 050102.M Fri May 17 15:07:29 2002 Page 9

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