GCMS scan report for Method 508, April 2002

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Data File : C:\MSDCHEM\1\DATA\020419\08430.D Vial: 17 Acq On : 19 Apr 2002 11:53 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 Phosphonic acid, dioctadecy... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 38.54 0.57 ug/1 1129750 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phosphonic acid, dioctadecyl ester 587 C36H7503P 019047-85-9 91. 2 3-Eicosene, (E)- 280 C20H40 074685-33-9 70 3 1-Docosene 308 C22H44 001599-67-3 64 4 2-Propenoic acid. n-tetradecyl e... 268 C17H3202 1000245-63-9 62 Abundance Scan 6036 (38.544 min): 08430.D (-6029) (-) m/z 55.05 100.00% 55

5000 69 83 97 4' 111 127 7 A*CAMAAAG , TYMPMAppatop4 38.20 38.40 38,60 38.80

n/z-> 01 mPH 20 40 ।60 _i । -ll‘,Il_ i'। i i ,ill 1 ill I ll hll rr 141 if 207 TWPmmumOTTD “]* । f । । । । । i j । 80 100 120 140 160 180 200 220 240 260 280 300 m/z 43.20 52.66% Abundance #13890: Phosphonic acid, dioctadecyl ester 55 69 83 4' 97 5000 MMWMMVWMM 111 38,20 38,40 38.60 38.80 136 m/z 57.10 51.10%| 0 ...ill ‘. । .ill. I, .1, 151.................................... , > 1111 ri 111 < । > ■ । > । ^ 11111111111 11' 111 11111111111111111

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #16986:3-Eicosene, (E)- 43 57 83 I bAus,./ "Man72At 97 38.20 38.40 38.60 38,80 5000 m/z 83.10 50.72%| 29 111 125 l | 139153167182196210224 252 280 0 TTT Ir । "14 111 । ""i 111.111111" 11111111111111111 < 111 —p n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #111438:1 -Docosene 41 55 38,20 38,40 38.60 38.80 69 83 97 m/z 69.10 49.00% 5000 111 2‘ 125

n/z-> 0 "‘I’ 20 4+1 Ir | 139153167181 Te 40 60 80 100 120 140 160 180 200 220 240 260 280 300 308 111 " 1' 11'111 " 1' I " " 1111' 38.20 38.40 38.60 38.80

08430.D SCAN020418.M Mon Apr 29 08:29:50 2002 Page 22

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