GCMS analysis results for sample AE10899, May 21 2002

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Data File : C:\MSDCHEM\l\DATA\051602\10899.D Vial: 12 Acq On : 16 May 2002 11:30 pm Operator: Mclean Sample : 5/10 eh Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 2H-Azepin-2-one, hexahydro-... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T. 30.10 0.90 ug/L 1059660 Chrysene-dl2 • 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Azepin-2-one, hexahydro-6-met... 127 C7H13NO 006142-55-8 9 2 3-Piperidinone, 1-methyl- 113 C6H11NO 005519-50-6/9 3 2H-Azepin-2-one, hexahydro-4-met... 127 C7H13NO 003623-05 9 4 Hexacosane 366 C26H54 000630-01-3 9 Abundance Scan 4598 (30.095 min): 10899.D (-4593) (-) m/z 57.10 100.00% 57 wwAlv/Yu-l 5000 43 69 80 94 113125 244

0 1 ■ i ■ 1 ,3,1145..165 29.80 30.00 30.20 30.40 m/z 43.10 39.96% mfe-> Abundance 20

33 40 60 120 140 #912:2H-Azepin-2-one, hexahydro-6-methyl- 160 180 200 220 240 4MWMy""hunsoh 98 42 55 69 127 5000 84 29.80 30.00 30.20 30.40 m/z 69.10 37.91% 15 O+ — | 112 j I ■ i" ■ i i" । i । । > । । । > ■ < । । । < * > । ■ । । ■ । ■ ■ । । । 1 > MWMWAMPWpw/"W miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #16218:3-Piperidinone, 1-methyl- 57 42 84 29.80 30.00 30.20 30.40 5000 113 m/z 125.10 24.56%

01 ■ ' i ■ ' ' ■ |l 1 '"' I 1 ' 1 1 I1' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #844: 2H-Azepin-2-one, hexahydro-4-methyl- 33 29.80 30.00 30.20 30.40 m/z 94.10 22.42% 69 43 127 5000 56

m/z-> 0 15. I , ' r I

20 '■ cl 40 .. al 60 80 83 - 98 112 100 TT" 0 120 140 160 180 200 220 240 "ri fl I ill 29.80 30.00 30.20 30.40

10899.D 050102.M Fri May 17 15:07:31 2002 Page 13

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