NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C : \HPCHEM\ 1 \DATA\MAYO 3 02 \LBA. D Vial: 15
Acq On 4 May 2002 3:46 am Operator:
Sample GC/MS SCAN 4/22 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.80 0.46 ug/1 38917 Naphthalene-d8 15.82
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72
2 N-(Trifludroacetyl)-N,0,0' ,0'1-tetr 553 C22H42F3NO4S14 000000-00-0 38
3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38
4 3,4-Dihy oxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38
Abundance Scan 1065 (14.798 min): LBA.D (-) m/z 73.05 100.00%!
73
5000
267 355
..................
45 14,40 14.60 14.80 15.00 15.20
— 154 191 ■ ■ ■ ■ i''1' i ■ ■' ■ i| '' ■' i' ■ ■ ■ i ■'' ■ i ■ ‘r ■ i ■'
1 ■■ । ■ rr" i m/z 267.05 37.07%|
m/z- > 50 100 150 200 250 300 350 400 450 500 550
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
5000
267 _ [110
14.40 14.60 14.80 15.00 15.20
m/z 355.10 35.89%|
—T
.............. 207 323,
mz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi
73
_ -------
355 14.40 14.60 14.80 15.00 15.20
5000 m/z 356.00 11.18%|
45
Lh
1 ‘i ' ■ '
147
.......... < 1 >
193 267
[■ । . . > । । i "i / । । .
L..................................... 538 , ,
m/z-> 50 100 150 200 250 350 300
400 450 500 550
Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls
73 14.40 14.60 14.80 15.00 15.20
m/z 267.95 9.33%
5000 355
44
it .
1'i
। .
■ ■ ' ■ i ■
147 193 267 294
m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
LBA.D GCMS0501.M Tue May 07 09:39:01 2002 Page 2
NYC-WTC_000023396
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