Liquid-liquid extraction log sheet, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\MAYO 3 02 \LBA. D Vial: 15 Acq On 4 May 2002 3:46 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 10.06 ug/1 684069 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C (O) OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexeh-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 341 (8.163 min): LBA.D (-) m/z 43.05 100.00% 43

5000 59

■ ■ i ■ ■ ■ ■ i ■ ■ 101 7.80 8.00 8.20 8.40 8.60 83 ..................................... ■ ■ i ■ ■ • ■ i ■ ■ ■ • i ■ ■ • ‘ f ■ 1.53.. —1——dd/—————/B////d/0 m/ z 59.10 42.52% miz-> 10 20 30 40 50 160 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 1 ■ i ■ ■ ■ ■ i ■ ' 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 16.90% 27 101

mz-> ------- 10 20 30 40 50 -I II 60 70 80 83 90 +49 । I,...... 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43

7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.72%

58 72 100 . ................................ .. ■ ' i - ■ ' ' ' i ■ 1 i ■ 1 ■ ■ i ■ ■ 1 ' I ■ ' 1 ' i '

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone ■ ■ i ' - - ■ i - ■ ■ * i ■ > < ■ i * • ■ ■ i ■ 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.15 7.17%

5000 15 58 27 r . , 4l . । , -1111 , r i 14 1 ' ■ I ' ' ■ 1 1 1 1 1 i 1 1 1 1 । 1 1 1 1 । 1 1 1 1 । 1 ■ 1 1 i 1 1610000 1"Pi /, । 1UUBT"CTu m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

LBA.D GCMS0501.M Tue May 07 09:39:00 2002 Page 1

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