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GCMS blank analysis results for sample AE08684, April 22, 2002

Machine-extracted title · confidence 100%

GCMS blank quality control report for sample AE08684 analyzed on April 22, 2002.

NYC-WTC_000048881–000048889

Folder label: “GCMS X 4/11/02 A 4/22/02

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Scanned page image, NYC-WTC_000048888
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2 2 02\LB.D Vial: 3 Acq On : 22 Apr 2002 11:06 am Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.19 6.19 ug/1 814486 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 Acetic acid, cyano-, 1,1-dimethylet 141 C7H11N02 001116-98-9 17 3 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 10 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 343 (8.191 min): LB.D (-) m/z 43.00 100.00% 43

59 5000 101 ■ i ■ ■ 1 ' i ■ m I ■ ' 7.80 8.00 8.20 8.40 8.60 1111'11 ■' ■ 'r1 +53+ ........ 371 71I 83 ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ' 1 i 1 1 ■ ■ i ' ‘ ‘ i ■ ' ■ ' i ■ 1 m/ z 59.05 53.17% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 ..... L..... 7.80 8.00 8.20 8.40 8.60 m/z 101.05 22.65% 27 , 1.., ,1, J. , , . ! | +49+ I 1 1 I ■ 1 1 ■ i ' ■ • ■ i 83 1 ■ i ■ 1 1 , 101I 1 i ■ ■ ■ ■ i ‘ ■ i • • ■ ■ i ■

iz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #7666: Acetic acid, cyano-, 1,1 -dimethylethyl ester 59 ' i 1 ■ ■ ■ i ■ ■ 7.80 8.00 8.20 8.40 8.60 5000 41 m/ z 58.05 16.91%

68 1...... .. 126 I " " I " ' 1 I'l — —mmmmmTTT miz-> 20 30 401 50 60 70 80 90 100 110 120 130 Abundance #1448: CH2=CHCH2C(O)OCH3 ■ i • ■ ■ ■ i ■ " 111 1 ■ ■ ■ i ■' 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.82%

5000

56 72 100 m/z-> 17737 20 30 40 ' I 1 ‘

50 60 I ‘ ‘ ‘ ‘ I I ' ■ ■ I ‘ ‘ ‘ ' I ' ' ' ■ I ' ‘

70 80 90 100 ' 1 ' ‘

110 ‘ I ' ' ' ‘ I ' ‘

120 130 1137 i 1 ■ 7.80 8.00 । । । 147 I ’IIt 8.20 8.40 8.60

NYC-WTC_000048888

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NYC-WTC_000048888Source: NYC Law Department, mirrored locally

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