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GCMS calibration data for TCLP method, May 2002

Machine-extracted title · confidence 100%

GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000022930–000022937

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022933
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\MAYO 302\9568.D Vial: 42 Acq On 5 May 2002 8:11 am Operator: Sample GC/MS SCAN 4/23 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.156 336 340 371 rBV 441690 965994 23.55% 4.613% 2 12.188 775 780 796 rBV 1269689 2911694 70.99% 13.903% 3 14.791 1058 1064 1071 rBV 221591 454504 11.08% 2.170% 4 15.826 1170 1177 1194 rBV 1781208 3686901 89.89% 17.605% 5 21.132 1748 1756 1777 rBV 1925565 4101708 100.00% 19.585%

6 23.267 1980 1989 1995 rVB 91077 185733 4.53% 0.887% 7 25.576 2234 2241 2251 rBV2 1787557 3799442 92.63% 18.142% 8 33.640 3113 3121 3137 rBV 1192130 2739317 66.78% 13.080% 9 37.865 3573 3582 3603 rBV2 702848 2097611 51.14% 10.016%

Sum of corrected areas: 20942904

9568.D GCMS0501.M Tue May 07 14:59:56 2002

NYC-WTC_000022933

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NYC-WTC_000022933Source: NYC Law Department, mirrored locally

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