GCMS calibration data for TCLP method, May 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Data File C:\HPCHEM\l\DATA\MAY0302\9570.D Vial: 44 Acq On 5 May 2002 10:09 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.158 336 340 368 rBV 430951 989995 24.55% 4.808% 2 12.190 772 780 796 rBV 1266290 2911636 72.21% 14.140% 3 14.792 1057 1064 1070 rBV 232263 462199 11.46% 2.245% 4 15.828 1171 1177 1194 rBV 1795994 3666001 90.92% 17.803% 5 21.133 1749 1756 1775 rBV 1929934 4032166 100.00% 19.581% 6 23.269 1981 1989 1995 rVB 120880 238845 5.92% 1.160% 7 25.578 2234 2241 2252 rBV2 1741504 3738625 92.72% 18.156% 8 33.633 3110 3120 3135 rBV2 1106417 2589657 64.22% 12.576% 9 37.866 3573 3582 3598 rBV2 659530 1962774 48.68% 9.532%

Sum of corrected areas: 20591898 9570.D GCMS0501.M Tue May 07 15:00:24 2002

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