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GCMS calibration results for sample AE09585, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS calibration data for sample AE09585 generated on May 4-6, 2002.

NYC-WTC_000046294–000046302

Folder label: “GCMS X 5/7/02 A 5/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAY0302\9585.D Vial: 12 Acq On 4 May 2002 12:49 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.156 336 340 346 rBV 412898 818261 23.13% 4.582% 2 8.229 346 348 372 rVB 43405 153848 4.35% 0.862% 3 12.188 775 780 797 rVB 1118814 2562887 72.45% 14.353% 4 14.791 1059 1064 1070 rVB 140056 280963 7.94% 1.573% 5 15.826 1171 1177 1187 rBV 1611639 3233291 91.40% 18.107%

6 21.132 1749 1756 1767 rBV 1716215 3537514 100.00% 19.811% 7 23.276 1982 1990 1997 rVB 132224 270752 7.65% 1.516% 8 25.576 2234 2241 2251 rBV2 1525990 3212702 90.82% 17.992% 9 33.640 3114 3121 3135 rBV2 932542 2151908 60.83% 12.051% 10 37.864 3573 3582 3599 rBV2 547030 1634568 46.21% 9.154%

Sum of corrected areas: 17856694

9585 .D GCMS0501.M Mon May 06 10:50:40 2002

NYC-WTC_000046297

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NYC-WTC_000046297Source: NYC Law Department, mirrored locally

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