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GCMS calibration results for sample AE09586, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS calibration data for sample AE09586 generated on May 4-6, 2002.

NYC-WTC_000046313–000046320

Folder label: “GCMS X 5/7/02 A 5/9/02

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Scanned page image, NYC-WTC_000046316
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0302\9586.D Vial: 13 Acq On 4 May 2002 1:48 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.165 337 341 370 rVB 462723 1066330 31.25% 6.154% 2 12.188 775 780 796 rVB 1064050 2436848 71.42% 14.063% 3 14.799 1059 1065 1070 rVB 81785 164668 4.83% 0.950% 4 15.826 1171 1177 1194 rBV 1521740 3091884 . 90.62% 17.843% 5 21.132 1750 1756 1769 rBV 1657878 3411870 100.00% 19.689%

6 23.267 1983 1989 1995 rBV 118330 245137 7.18% 1.415% 7 25.576 2234 2241 2252 rBV2 1504820 3134455 91.87% 18.088% 8 33.631 3114 3120 3135 rBV2 926368 2135599 62.59% 12.324% 9 33.860 3141 3145 3154 rVB 15928 40393 1.18% 0.233% 10 37.864 3573 3582 3597 rBV2 556942 1601456 46.94% 9.242%

Sum of corrected areas: 17328640

9586.D GCMS0501.M Mon May 06 10:50:55 2002

NYC-WTC_000046316

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NYC-WTC_000046316Source: NYC Law Department, mirrored locally

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