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GCMS results for sample AE09654, May 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AE09654 conducted on May 23, 2002, showing surrogate recovery data.

NYC-WTC_000023754–000023767

Folder label: “GCMS X 5/9/02 A 5/20/02

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Scanned page image, NYC-WTC_000023765
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAY0602\9673.D Vial: 13 Acq On 7 May 2002 4:03 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.163 337 341 361 rBV 301708 708229 15.28% 3.101% 2 12.195 775 781 798 rBV 1437658 3295114 71.08% 14.430% 3 15.832 1171 1178 1195 rBV 1943821 4176228 90.08% 18.289% 4 21.138 1750 1757 1773 rBV 2171282 4635890 100.00% 20.301% 5 23.273 1983 1990 1996 rBV 157528 311443 6.72% 1.364%

6 25.583 2234 2242 2253 rBV2 1958379 4394070 94.78% 19.242% 7 33.637 3114 3121 3137 rBV2 1351545 3041974 65.62% 13.321% 8 33.857 3141 3145 3156 rVB 19663 50623 1.09% 0.222% 9 37.871 3572 3583 3603 rBV 753760 2221682 47.92% 9.729%

Sum of corrected areas: 22835253

9673.D GCMS0501.M Wed May 08 14:01:48 2002

NYC-WTC_000023765

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NYC-WTC_000023765Source: NYC Law Department, mirrored locally

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