GCMS calibration data for TCLP method, May 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0 3 02\9569.D Vial: 43 Acq On 5 May 2002 9:10 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.163 337 341 370 rBV 424296 980305 24.33% 4.655% 2 12.195 775 781 799 rBV 1267949 2892815 71.79% 13.737% 3 14.797 1058 1065 1072 rBV 156957 308015 7.64% 1.463% 4 15.823 1171 1177 1194 rBV 1780006 3674087 91.17% 17.447% 5 21.129 1750 1756 1773 rBV 1837412 4029795 100.00% 19.136%

6 23.273 1983 1990 1997 rBV 149729 295940 7.34% 1.405% 7 25.573 2235 2241 2251 rBV2 1688761 3767719 93.50% 17.892% 8 33.637 3114 3121 3139 rBV 1253844 2807121 69.66% 13.330% 9 33.857 3139 3145 3152 rVB3 18917 51267 1.27% 0.243% 10 37.871 3574 3583 3602 rBV2 741289 2251366 55.87% 10.691%

Sum of corrected areas: 21058430

9569.D GCMS0501.M Tue May 07 15:00:10 2002

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