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GCMS results for sample AE10065, May 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AE10065 conducted on May 23, 2002, showing surrogate recovery data.

NYC-WTC_000023738–000023744

Folder label: “GCMS X 5/9/02 A 5/20/02

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Scanned page image, NYC-WTC_000023741
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0302\10065.D Vial: 38 Acq On 5 May 2002 4:16 am Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.155 337 340 346 rBV 483522 945970 23.55% 4.603% 2 12.196 775 781 797 rBV 1251150 2873587 71.54% 13.981% 3 15.825 1171 1177 1195 rBV 1761288 3651334 90.91% 17.765% 4 21.131 1750 1756 1771 rBV 1887924 4016555 100.00% 19.542% 5 23.275 1984 1990 1996 rBV 113947 228955 5.70% 1.114%

6 25.575 2234 2241 2252 rBV2 1701547 3701844 92.16% 18.011% 7 33.639 3114 3121 3132 rBV 1204646 2671943 66.52% 13.000% 8 33.859 3139 3145 3161 rVB 175453 400530 9.97% 1.949% 9 37.863 3573 3582 3603 rBV2 689180 2062523 51.35% 10.035%

Sum of corrected areas: 20553241

10065.D GCMS0501.M Tue May 07 12:00:58 2002

NYC-WTC_000023741

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NYC-WTC_000023741Source: NYC Law Department, mirrored locally

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