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GCMS calibration results for sample AE09580, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS calibration data for sample AE09580 generated on May 3-6, 2002.

NYC-WTC_000046276–000046283

Folder label: “GCMS X 5/7/02 A 5/9/02

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Scanned page image, NYC-WTC_000046279
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAY0302\9580.D Vial: 10 Acq On 3 May 2002 10:51 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.158 336 340 346 rBV 481172 926112 24.26% 4.805% 2 12.190 774 780 795 rVB 1260120 2747944 71.98% 14.258% 3 14.792 1059 1064 1069 rVB 91138 173818 4.55% 0.902% 4 15.828 1170 1177 1193 rBV 1696332 3483385 91.25% 18.074% 5 21.133 1749 1756 1772 rBV 1841482 3817505 100.00% 19.808%

6 23.268 1983 1989 1995 rBV 81679 159599 4.18% 0.828% 7 25.578 2234 2241 2251 rBV2 1661043 3493564 91.51% 18.127% 8 33.642 3114 3121 3134 rBV2 1091598 2497421 65.42% 12.958% 9 37.866 3573 3582 3601 rBV2 662568 1973144 51.69% 10.238%

Sum of corrected areas: 19272492

9580.D GCMS0501.M Mon May 06 10:50:10 2002

NYC-WTC_000046279

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NYC-WTC_000046279Source: NYC Law Department, mirrored locally

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