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GCMS results for sample AE09676, May 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AE09676 conducted on May 23, 2002, showing surrogate recovery data.

NYC-WTC_000023811–000023827

Folder label: “GCMS X 5/9/02 A 5/20/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File C: \HPCHEM\ 1 \DATA\MAYO 602\9676.D Vial: 19 Acq On 7 May 2002 9:55 am Operator: Sample GC/MS SCAN 4/25 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.158 336 340 369 rBV 476660 1048710 19.18% 4.004% 2 12.190 774 780 796 rBV 1707964 3888529 71.13% 14.848% 3 15.828 1170 1177 1193 rBV 2356081 4911715 89.85% 18.755% 4 21.134 1749 1756 1779 rBV 2525623 5466871 100.00% 20.874% 5 23.269 1982 1989 1995 rBV 170043 340791 6.23% 1.301% 6 25.578 2233 2241 2252 rBV2 2342237 5073318 92.80% 19.372% 7 33.633 3113 3120 3139 rBV2 1369030 3205941 58.64% 12.241% 8 37.866 3573 3582 3600 rBV2 745070 2253472 41.22% 8.605%

Sum of corrected areas: 26189347 9676.D GCMS0501.M Thu May 09 11:25:06 2002

NYC-WTC_000023814

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NYC-WTC_000023814Source: NYC Law Department, mirrored locally

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