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GCMS calibration results for sample AE09587, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS calibration data for sample AE09587 generated on May 4-6, 2002.

NYC-WTC_000046332–000046339

Folder label: “GCMS X 5/7/02 A 5/9/02

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Scanned page image, NYC-WTC_000046335
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0302\9587.D Vial: 14 Acq On 4 May 2002 2:47 am Operator: Sample GC/MS SCAN 4/24 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.161 337 341 370 rVB 463053 994635 34.71% 6.920% 2 12.193 775 781 801 rVB 941764 2065237 72.08% 14.368% 3 14.796 1060 1065 1070 rBV 46077 85574 2.99% 0.595% 4 15.831 1172 1178 1193 rVB 1228479 2597225 90.64% 18.069% 5 21.137 1750 1757 1770 rBV 1347763 2865279 100.00% 19.934%

6 23.272 1982 1990 1996 rBV 102173 196887 6.87% 1.370% 7 25.572 2235 2241 2252 rBV2 1222307 2554376 89.15% 17.771% 8 33.636 3115 3121 3139 rBV 765302 1706682 59.56% 11.873% 9 37.861 3574 3582 3600 rBV2 443128 1308160 45.66% 9.101%

Sum of corrected areas: 14374055

9587.D GCMS0501.M Mon May 06 10:51:09 2002

NYC-WTC_000046335

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NYC-WTC_000046335Source: NYC Law Department, mirrored locally

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