Volatile organic compounds blank results, Feb 28 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02FEB28\0228C10.D Vial: 2 Acq On : 28 Feb 2002 9:34 am Operator: Sample : cal 10 Inst : 210 Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: GAS5.P Quant Time: Feb 28 10:23 2002 Quant Results File: HP021102.RES Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Last Update : Thu Feb 28 10:22:51 2002 Response via : Initial Calibration DataAcq Meth : HP021102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 714091 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.34 82 388340 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE-D4 29.40 152 323368 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-Diehloroethane-d4 14.64 65 168954 5.58 ug/L 0.00 Spiked Amount 5.000 Recovery = 111.60% 22) Toluene-d8 19.49 98 930169 4.74 ug/L 0.00 Spiked Amount 5.000 Recovery = 94.80% 50) 4-Bromofluorobenzene 26.40 95 346930 5.14 ug/L 0.02 Spiked Amount 5.000 Recovery = 102.80% Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.21 85 447615 9.45 ug/L 100 4) CHLOROMETHANE 4.81 50 428161 10.61 ug/L 96 5) VINYL CHLORIDE 4.89 62 625001 12.34 ug/L 99 6) BROMOMETHANE 5.74 96 278109 8.52 ug/L 100 7) CHLOROETHANE 5.87 64 300640 9.51 ug/L 97 8) TRICHLOROFLUOROMETHANE 6.39 101 580381 12.35 ug/L 99 9) ACETONE 8.04 43 6452 7.98 ug/L 85 10) 1,1-DICHLOROETHENE 7.78 61 500121 7.53 ug/L 95 11) METHYLENE CHLORIDE 8.97 49 567405 9.15 ug/L 96 12) METHYL TERT BUTYL ETHER 9.29 73 900020 10.73 ug/L 98 13) TRANS-1,2-DICHLOROETHENE 9.74 61 698282 10.29 ug/L 96 14) 1,1-DICHLOROETHANE 10.82 63 877856 10.66 ug/L 99 15) 2-BUTANONE (MEK) 12.27 43 49632 16.12 ug/L 95 16) 2,2-DICHLOROPROPANE 12.26 77 729979 12.13 ug/L 97 17) CIS-1,2-DICHLOROETHENE 12.40 61 713887 11.06 ug/L 94 18) CHLOROFORM 12.79 83 885582 11.22 ug/L 100 19) BROMOCHLOROMETHANE 13.24 49 326507 10.90 ug/L 90 20) 1,2-DICHLOROETHANE 16.91 62 382254 11.26 ug/L 98 23) 1,1,1-TRICHLOROETHANE 13.83 97 705950 10.65 ug/L 99 24) 1,1-DICHLOROPROPENE 14.24 75 723300 10.28 ug/L 99 25) CARBON TETRACHLORIDE 14.50 117 503998 10.27 ug/L 99 26) BENZENE 14.93 77 556935 9.64 ug/L 96 27) TRICHLOROETHENE 16.47 95 557123 10.20 ug/L 99 28) 1,2-DICHLOROPROPANE 16.91 63 539303 10.26 ug/L 98 29) DIBROMOMETHANE 17.67 174 167796 10.00 ug/L 98 30) BROMODICHLOROMETHANE 17.51 83 548688 10.27 ug/L 99 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 195813 11.02 ug/L 99

(#) = qualifier out of range (m) = manual integration 0228C10.D HP021102.M Thu Feb 28 10:23:30 2002 Page 1

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