VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02feb15\0215C10.D Vial: 2 Acq On : 15 Feb 2002 9:12 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise : February.15, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 15 9:50 2002 Quant Results File: HP021302.RES Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Feb 15 09:42:18 2002 Response via : Initial Calibration DataAcq Meth : HP021302

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.06 114 2038101 5.00 ug/L -0.05 24) CHLOROBENZENE-D5 21.71 117 2010690 5.00 ug/L -0.05 52) 1,4-DICHLOROBENZENE-D4 26.90 152 948059 5.00 ug/L -0.05 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.29 65 745669 4.81 ug/L -0.05 Spiked Amount 5.000 Recovery = 96.20% 3) 4-BROMOFLUOROBENZENE 24.30 174 712403 4.65 ug/L -0.05 Spiked Amount 5.000 Recovery = 93.00% 25) TOLUENE-D8 18.42 98 2503275 5.02 ug/L -0.05 Spiked Amount 5.000 Recovery = 100.40% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.83 85 531670 7.40 ug/L 98 5) CHLOROMETHANE 5.47 50 475412 8.64 ug/L 99 6) VINYL CHLORIDE 5.55 62 183247 7.58 ug/L 99 7) BROMOMETHANE 6.54 94 261573 7.88 ug/L 99 8) CHLOROETHANE 6.69 64 247798 7.39 ug/L 98 9) TRICHLOROFLUOROMETHANE 7.25 101 463249 7.19 ug/L 99 10) Isopropyl Alcohol 7.85 45 1392099 998.03 ug/L 94 11) 1,1,2-Trichloro-1,2,2-trif 8.13 101 396784 7.65 ug/L 95 12) ACETONE 8.22 43 172631 12.32 ug/L 94 13) 1,1-DICHLOROETHENE 8.57 61 1064376 10.87 ug/L 99 14) METHYLENE CHLORIDE 9.58 49 1383681 11.75 ug/L 93 15) METHYL TERT BUTYL ETHER 9.87 73 1264160 9.72 ug/L 93 16) TRANS-1,2-DICHLOROETHENE 10.24 61 1269385 10.13 ug/L 94 17) 1,1-DICHLOROETHANE 11.13 63 1466059 9.90 ug/L 97 18) 2-BUTANONE (MEK) 11.96 43 389671 12.00 ug/L 96 19) 2,2-DICHLOROPROPANE 12.34 77 1091039 9.18 ug/L 97 20) CIS-1,2-DICHLOROETHENE 12.43 96 860540 10.17 ug/L 95 21) CHLOROFORM 12.78 83 1448765 9.74 ug/L 99 22) BROMOCHLOROMETHANE 13.16 49 772093 10.91 ug/L 97 23) 1,2-DICHLOROETHANE 14.50 62 959449 9.58 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.67 97 1081079 9.64 ug/L 97 27) 1,1-DICHLOROPROPENE 14.00 75 1143034 10.22 ug/L 99 28) CARBON TETRACHLORIDE 14.26 117 901965 9.89 ug/L 99 29) BENZENE 14.59 78 2971658 10.23 ug/L 100 30) TRICHLOROETHENE 15.86 95 890768 10.26 ug/L 97 31) 1,2-DICHLOROPROPANE 16.23 63 901855 10.99 ug/L 97 32) DIBROMOMETHANE 16.89 174 424940 10.90 ug/L 99 33) BROMODICHLOROMETHANE 16.73 83 1061717 10.11 ug/L 99 (#) = qualifier out of range (m) = manual integration 0215C10.D HP021302.M Fri Feb 15 09:50:45 2002 Page 1

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