VOC analysis results, sample AE03934, Feb 27 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02FEB27\0227C10.D Vial: 3 Acq On : 27 Feb 2002 10:18 am Operator: Sample : cal 10 Inst : 210 Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Feb 27 11:22 2002 Quant Results File: HP021102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Wed Feb 27 11:22:25 2002 Response via : Initial Calibration DataAcq Meth : HP021102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 777312 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.34 82 425058 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE-D4 29.39 152 393724 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-Dichioroethane -d4 14.64 65 215248 6.53 ug/L 0.00 Spiked Amount 5.000 Recovery = 130.60% 22) Toluene-d8 19.49 98 1001848 4.66 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.20% 50) 4-Bromofluorobenzene 26.39 95 398876 4.85 ug/L 0.00 Spiked Amount 5.000 Recovery = 97.00%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.21 85 583441 11.48 ug/L 100 4) CHLOROMETHANE 4.78 50 557948 12.70 ug/L 98 5) VINYL CHLORIDE 4.89 62 789604 14.49 ug/L 98 6) BROMOMETHANE 5.74 96 386403 10.88 ug/L 96 7) CHLOROETHANE 5.87 64 419719 12.19 ug/L 98 8) TRICHLOROFLUOROMETHANE 6.40 101 808110 15.79 ug/L 97 9) ACETONE 8.04 43 12543 14.25 ug/L 85 10) 1,1-DICHLOROETHENE 7.78 61 697829 9.65 ug/L 94 11) METHYLENE CHLORIDE 8.97 49 855463 12.67 ug/L 90 12) METHYL TERT BUTYL ETHER 9.29 73 1050322 11.51 ug/L 96 13) TRANS-1,2-DICHLOROETHENE 9.73 61 771500 10.45 ug/L 94 14) 1,1-DICHLOROETHANE 10.82 63 969764 10.82 ug/L 100 15) 2-BUTANONE (MEK) 12.14 43 25150 10.80 ug/L 95 16) 2,2-DICHLOROPROPANE 12.26 77 763165 11.65 ug/L 99 17) CIS-1,2-DICHLOROETHENE 12.40 61 777604 11.07 ug/L 94 18) CHLOROFORM 12.79 83 968105 11.27 ug/L 99 19) BROMOCHLOROMETHANE 13.25 49 386700 11.85 ug/L 93 20) 1,2-DICHLOROETHANE 16.91 62 417236 11.29 ug/L 100 23) 1,1,1-TRICHLOROETHANE 13.82 97 741127 10.22 ug/L 98 24) 1,1-DICHLOROPROPENE 14.22 75 762438 9.90 ug/L 97 25) CARBON TETRACHLORIDE 14.50 117 519237 9.67 ug/L 99 26) BENZENE 14.92 77 590712 9.34 ug/L 97 27) TRICHLOROETHENE 16.47 95 571562 9.56 ug/L 99 28) 1,2-DICHLOROPROPANE 16.91 63 585404 10.18 ug/L 99 29) DIBROMOMETHANE 17.67 174 197545 10.76 ug/L 96 30) BROMODICHLOROMETHANE 17.51 83 600456 10.27 ug/L 98 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 206861 10.63 ug/L # 92

(#) = qualifier out of range (m) = manual integration 0227C10.D HP021102.M Wed Feb 27 11:23:05 2002 Page 1

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