Volatile organic compounds blank results, Mar 1 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02MAR01\0301C10A.D Vial: 18 Acq On : 2 Mar 2002 12:34 am Operator: Sample : cal 10 Inst : 210 Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: GAS5.P Quant Time: Mar 4 11:24 2002 Quant Results File: HP021102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Mar 04 11:23:12 2002 Response via : Initial Calibration DataAcq Meth : HP021102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 831265 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.34 82 406928 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE-D4 29.39 152 333441 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,2-Dichloroethane-d4 14.63 65 196154 5.56 ug/L 0.00 Spiked Amount 5.000 Recovery = 111.20% 22) Toluene-d8 19.49 98 1046288 5.09 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.80% 50) 4-Bromofluorobenzene 26.39 95 360584 5.18 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.60%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.22 85 357474 8.56 ug/L 97 4) CHLOROMETHANE 4.83 50 392843 8.36 ug/L 97 5) VINYL CHLORIDE 4.90 62 595144 9.96 ug/L 99 6) BROMOMETHANE 5.75 96 292341 7.69 ug/L 95 7) CHLOROETHANE 5.88 64 392992 10.68 ug/L 98 8) TRICHLOROFLUOROMETHANE 6.41 101 684259 12.50 ug/L 98 9) ACETONE 8.07 43 9751 10.36 ug/L 99 10) 1,1-DICHLOROETHENE 7.79 61 636866 8.23 ug/L 93 11) METHYLENE CHLORIDE 8.98 49 668212 9.26 ug/L 90 12) METHYL TERT BUTYL ETHER 9.29 73 843699 8.64 ug/L 98 13) TRANS-1,2-DICHLOROETHENE 9.73 61 734842 9.30 ug/L 94 14) 1,1-DICHLOROETHANE 10.82 63 950729 9.92 ug/L 98 15) 2-BUTANONE (MEK) 12.26 43 40479 13.39 ug/L 95 16) 2,2-DICHLOROPROPANE 12.26 77 641498 9.16 ug/L 98 17) CIS-1,2-DICHLOROETHENE 12.40 61 760042 10.12 ug/L 94 18) CHLOROFORM 12.79 83 914472 9.95 ug/L 100 19) BROMOCHLOROMETHANE 13.25 49 354162 10.15 ug/L 90 20) 1,2-DICHLOROETHANE 16.91 62 386958 9.79 ug/L 99 23) 1,1,1-TRICHLOROETHANE 13.83 97 723489 10.42 ug/L 99 24) 1,1-DICHLOROPROPENE 14.22 75 741008 10.05 ug/L 96 25) CARBON TETRACHLORIDE 14.50 117 508294 9.89 ug/L 99 26) BENZENE 14.93 77 559754 9.25 ug/L 98 27) TRICHLOROETHENE 16.47 95 560476 9.79 ug/L 99 28) 1,2-DICHLOROPROPANE 16.91 63 544662 9.89 ug/L 99 29) DIBROMOMETHANE 17.67 174 165508 9.42 ug/L 98 30) BROMODICHLOROMETHANE 17.50 83 531544 9.50 ug/L 98 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 201437 10.82 ug/L 90

(#) = qualifier out of range (m) = manual integration 0301C10A.D HP021102.M Mon Mar 04 11:30:12 2002 Page 1

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