VOCs GC/MS analysis results, Jan 22-23 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02jan22\0122C10A.D Vial: 9 Acq On : 22 Jan 2002 3:26 pm Operator: Sample : cal 10 Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 22 16:07 2002 Quant Results File: HP010802.RES

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Jan 17 13:37:20 2002 Response via : Initial Calibration DataAcq Meth : HP010802

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 17.56 114 711438 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 25.15 82 405283 5.00 ug/L -0.01 49) 1,4-DICHLOROBENZENE-D4 31.12 152 328282 5.00 ug/L -0.01

System Monitoring Compounds 2) 1,2-Dichloroethane-d4 16.59 65 157098 4.63 ug/L -0.01 Spiked Amount 5.000 Recovery = 92.60% 22) Toluene-d8 21.40 98 924771 4.91 0.00 ug/L

Spiked Amount 5.000 Recovery = 98.20% 50) 4-Bromofluorobenzene 28.16 95 353731 5.14 0.00 ug/L

Spiked Amount 5.000 Recovery = 102.80%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.33 85 516804 18.68 100 ug/L

4) CHLOROMETHANE 5.03 50 497364 15.54 98 ug/L

5) VINYL CHLORIDE 5.19 62 552745 13.59 100 ug/L

6) BROMOMETHANE 6.32 96 331999 13.77 97 ug/L

7) CHLOROETHANE 6.53 64 376026 15.96 99ug/L

8) TRICHLOROFLUOROMETHANE 7.26 101 625617 13.09 97ug/L

9) ACETONE 9.31 43 7591 4.74 100 ug/L

10) 1,1-DICHLOROETHENE 9.10 61 957564 12.41 ug/L 98 11) METHYLENE CHLORIDE 10.55 49 809153 11.68 ug/L 97 12) METHYL TERT BUTYL ETHER 10.97 73 1015478 11.95 99 ug/L

13) TRANS-1,2-DICHLOROETHENE 11.40 61 949149 11.98 ug/L 97 14) 1,1-DICHLOROETHANE 12.62 63 1183229 12.45 ug/L 98 15) 2-BUTANONE (MEK) 14.03 43 27376 5.98 ug/L 92 16) 2,2-DICHLOROPROPANE 14.15 77 934010 12.03 ug/L 98 17) CIS-1,2-DICHLOROETHENE 14.29 61 918712 11.89 98 ug/L

18) CHLOROFORM 14.70 83 1118903 11.62 ug/L

99 19) BROMOCHLOROMETHANE 15.17 49 411055 11.75 ug/L 97 20) 1,2-DICHLOROETHANE 16.83 62 577028 11.49 ug/L 98 23) 1,1,1-TRICHLOROETHANE 15.76 97 898046 11.97 ug/L 99 24) 1,1-DICHLOROPROPENE 16.17 75 926764 12.45 ug/L

100 25) CARBON TETRACHLORIDE 16.43 117 638908 12.89 ug/L

100 26) BENZENE 16.87 77 704881 11.97 ug/L

100 27) TRICHLOROETHENE 18.41 95 702246 12.09 ug/L

99 28) 1,2-DICHLOROPROPANE 18.85 63 640090 12.02 ug/L

99 29) DIBROMOMETHANE 19.60 174 203627 11.85 ug/L 94 30) BROMODICHLOROMETHANE 19.44 83 670527 12.33 ug/L 98 31) 2-CHLOROETHYL VINYL ETHER 20.20 63 194927 13.47 ug/L 97 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0122C10A.D HP010802.M Tue Jan 22 16:08:06 2002 Page 1

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