SB1524 volatile analysis results, sample AEO1636, Jan 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02JAN28\0128C10.D Vial: 4 Acq On : 28 Jan 2002 12:23 pm Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise : January 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 28 16:38 2002 Quant Results File: HP010702.RES Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Last Update : Mon Jan 28 16:35:43 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.12 114 1020555 5.00 ug/L -0.05 24) CHLOROBENZENE-D5 21.78 117 873408 5.00 ug/L -0.07 52) 1,4-DICHLOROBENZENE-D4 26.95 152 428480 5.00 ug/L -0.07 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 618031 4.67 ug/L -0.07 Spiked Amount 5.000 Recovery = 93.40% 3) 4-BROMOFLUOROBENZENE 24.36 174 338035 4.89 ug/L -0.07 Spiked Amount 5.000 Recovery = 97.80% 25) TOLUENE-D8 18.47 98 1184200 5.09 ug/L -0.07 Spiked Amount 5.000 Recovery = 101.80% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.89 85 614451 13.74 ug/L 100 5) CHLOROMETHANE 5.47 50 495115 9.97 ug/L 95 6) VINYL CHLORIDE 5.61 62 497552 12.13 ug/L 95 7) BROMOMETHANE 6.62 94 362584 11.18 ug/L 96 8) CHLOROETHANE 6.75 64 284763 9.91 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.30 101 978638 12.08 ug/L 100 10) Isopropyl Alcohol 7.89 45 849597 769.97 ug/L 91 11) 1,1,2-Trichloro-l,2,2-trif 8.19 101 648286 12.10 ug/L - 96 12) ACETONE 8.27 43 116242 8.78 ug/L 96 13) 1,1-DICHLOROETHENE 8.62 61 937130 11.56 ug/L 97 14) METHYLENE CHLORIDE 9.63 49 961719 10.24 ug/L 99 15) METHYL TERT BUTYL ETHER 9.93 73 571687 10.42 ug/L 97 16) TRANS-1,2-DICHLOROETHENE 10.29 61 917302 11.42 ug/L 97 17) 1,1-DICHLOROETHANE 11.18 63 971259 11.01 ug/L 99 18) 2-BUTANONE (MEK) 12.02 43 180549 10.39 ug/L 99 19) 2,2-DICHLOROPROPANE 12.40 77 730688 11.84 ug/L 97 20) CIS-1,2-DICHLOROETHENE 12.49 96 505740 11.29 ug/L 95 21) CHLOROFORM 12.84 83 1116732 11.07 ug/L 97 22) BROMOCHLOROMETHANE 13.20 49 477278 9.38 ug/L 99 23) 1,2-DICHLOROETHANE 14.55 62 866806 10.35 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.73 97 991286 12.45 ug/L 99 27) 1,1-DICHLOROPROPENE 14.04 75 761279 12.34 ug/L 98 28) CARBON TETRACHLORIDE 14.30 117 1021396 12.76 ug/L 99 29) BENZENE 14.65 78 1751512 10.94 ug/L 99 30) TRICHLOROETHENE 15.92 95 565641 11.52 ug/L 96 31) 1,2-DICHLOROPROPANE 16.27 63 463479 10.08 ug/L 98 32) DIBROMOMETHANE 16.95 174 206366 10.16 ug/L 96 33) BROMODICHLOROMETHANE 16.79 83 727672 10.70 ug/L 97 (#) = qualifier out of range (m) = manual integration 0128C10.D HP010702.M Thu Feb 14 09:06:01 2002 Page 1

NYC-WTC_000019183