Volatile organic compounds blank results, Mar 1 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02MAR01\0301C10.D Vial: 3 Acq On : 1 Mar 2002 11:03 am Operator: Sample : cal 10 Inst : 210 Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: GAS5.P Quant Time: Mar 1 12:06 2002 Quant Results File: HP021102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Feb 28 12:27:24 2002 Response via : Initial Calibration DataAcq Meth : HP021102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 767492 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.34 82 429892 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE-D4 29.39 152 377942 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,2-Dichloroethane-d4 14.63 65 176988 5.43 ug/L 0.00 Spiked Amount 5.000 Recovery = 108.60% 22) Toluene-d8 19.49 98 998093 4.59 ug/L 0.00 Spiked Amount 5.000 Recovery = 91.80% 50) 4-Bromofluorobenzene 26.39 95 393180 4.98 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.60%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.21 85 212834 4.02 ug/L 99 4) CHLOROMETHANE 4.85 50 290835 6.70 ug/L 95 5) VINYL CHLORIDE 4.89 62 445297 7.98 ug/L 100 6) BROMOMETHANE 5.74 96 236876 6.75 ug/L 95 7) CHLOROETHANE 5.87 64 243502 7.17 ug/L 99 8) TRICHLOROFLUOROMETHANE 6.39 101 446261 8.83 ug/L 100 9) ACETONE 8.05 43 7203 8.29 ug/L 94 10) 1,1-DICHLOROETHENE 7.79 61 579883 8.12 ug/L 93 11) METHYLENE CHLORIDE 8.97 49 739769 11.10 ug/L 95 12) METHYL TERT BUTYL ETHER 9.29 73 868204 9.63 ug/L 98 13) TRANS-1,2-DICHLOROETHENE 9.73 61 683160 9.37 ug/L 93 14) 1,1-DICHLOROETHANE 10.82 63 878651 9.93 ug/L 99 15) 2-BUTANONE (MEK) 12.09 43 25793 11.02 ug/L 99 16) 2,2-DICHLOROPROPANE 12.26 77 692130 10.70 ug/L 98 17) CIS-1,2-DICHLOROETHENE 12.40 61 716149 10.33 ug/L 95 18) CHLOROFORM 12.79 83 860641 10.15 ug/L 99 19) BROMOCHLOROMETHANE 13.25 49 338186 10.50 ug/L 92 20) 1,2-DICHLOROETHANE 16.90 62 370754 10.16 ug/L 97 23) 1,1,1-TRICHLOROETHANE 13.82 97 656356 8.95 ug/L 98 24) 1,1-DICHLOROPROPENE 14.24 75 679303 8.72 ug/L 99 25) CARBON TETRACHLORIDE 14.50 117 462682 8.52 ug/L 99 26) BENZENE 14.92 77 532049 8.32 ug/L 98 27) TRICHLOROETHENE 16.47 95 525230 8.68 ug/L 99 28) 1,2-DICHLOROPROPANE 16.91 63 523245 8.99 ug/L 98 29) DIBROMOMETHANE 17.67 174 163982 8.83 ug/L 96 3 0) BROMODICHLOROMETHANE 17.50 83 518570 8.77 ug/L 99 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 186866 9.50 ug/L 92

(#) = qualifier out of range (m) = manual integration 0301C10.D HP021102.M Fri Mar 01 12:06:57 2002 Page 1

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