Volatile organic compounds blank results, Mar 1 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02MAR01\0301R5.D Vial: 4 Acq On : 1 Mar 2002 12:33 pm Operator: Sample : ref 5 Inst : 210 Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: GAS5.P Quant Time: Mar 1 14:19 2002 Quant Results File: HP021102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Mar 01 14:18:55 2002 Response via : Initial Calibration DataAcq Meth : HP021102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 752875 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.33 82 431767 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE-D4 29.40 152 352945 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,2-Dichloroethane-d4 14.63 65 175415 5.49 ug/L 0.00 Spiked Amount 5.000 Recovery = 109.80% 22) Toluene-d8 19.49 98 964342 4.42 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.40% 50) 4-Bromofluorobenzene 26.40 95 368435 5.00 ug/L 0.02 Spiked Amount 5.000 Recovery = 100.00%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.21 85 148456 3.93 ug/L 98 4) CHLOROMETHANE 4.87 50 172216 4.05 ug/L 99 5) VINYL CHLORIDE 4.89 62 248008 4.45 ug/L 98 6) BROMOMETHANE 5.75 96 127861 3.72 ug/L 97 7) CHLOROETHANE 5.87 64 129178 3.88 ug/L 98 8) TRICHLOROFLUOROMETHANE 6.39 101 227264 4.59 ug/L 98 10) 1,1-DICHLOROETHENE 7.78 61 306414 4.37 ug/L 95 11) METHYLENE CHLORIDE 8.97 49 264715 4.05 ug/L 95 12) METHYL TERT BUTYL ETHER 9.29 73 462593 5.23 ug/L 99 13) TRANS -1,2-DICHLOROETHENE 9.73 61 362608 5.07 ug/L 93 14) 1,1-DICHLOROETHANE 10.81 63 455003 5.24 ug/L 99 15) 2-BUTANONE (MEK) 12.26 43 12966 7.72 ug/L 79 16) 2,2-DICHLOROPROPANE 12.26 77 351570 5.54 ug/L 97 17) CIS-1,2-DICHLOROETHENE 12.39 61 356798 5.24 ug/L 94 18) CHLOROFORM 12.79 83 425730 5.12 ug/L 100 19) BROMOCHLOROMETHANE 13.25 49 171270 5.42 ug/L 96 20) 1,2-DICHLOROETHANE 16.91 62 188273 5.26 ug/L 98 23) 1,1,1-TRICHLOROETHANE 13.82 97 330431 4.49 ug/L 99 24) 1,1-DICHLOROPROPENE 14.24 75 354309 4.53 ug/L 99 25) CARBON TETRACHLORIDE 14.49 117 228055 4.18 ug/L 97 26) BENZENE 14.93 77 276812 4.31 ug/L 98 27) TRICHLOROETHENE 16.47 95 266643 4.39 ug/L 98 28) 1,2-DICHLOROPROPANE 16.91 63 261834 4.48 ug/L 99 29) DIBROMOMETHANE 17.67 174 80739 4.33 ug/L 91 30) BROMODICHLOROMETHANE 17.51 83 252793 4.26 ug/L 96 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 94682 4.79 ug/L # 93 32) METHYL ISO-BUTYL KETONE 18.35 58 28380 3.66 ug/L 72

(#) = qualifier out of range (m) = manual integration 0301R5.D HP021102.M Fri Mar 01 14:20:38 2002 Page 1

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