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GCMS blank analysis for sample AD30694, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.

NYC-WTC_000018069–000018092

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Silane, [1,2,3-benzenetriyltri Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.45 6.39 ug/1 2406900 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane, [1.2, 3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 16 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 16 3 1,1,1 5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 4 Cyclohexasiloxane, dodecamethyl - 444 C12H3606Si6 000540-97-6 10 Abundance Scan 1351 (17.449 min): LBD.D (-) m/z 73.00 100.00% 73

5000

147 341 429 17.20 17.40 17.60 17.80 _m miz-> 0- .45.A,.86,117..Tmpmm [ 179 207225 251 281 311 1 k i < ।. t .11. n. । n.. p... ।.... 397 . 11 > i, । ■ n 111 m/z 341.00 । I 27.06% 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris(trimethyl- 73 i 239 5000 342 ‘ t4***1*++*}‘4‘I4* 17.20 17.40 17.60 17.80 45 m/z 147.00 14.53% 133 179 211 .................... ................................. ........ | 4 ....................................... miz-> 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 " Abundance 73 #48337: 2H-1,4-Benzodiazepin-2-one, 7-cnloro-1.3-dinydro-5- 341 .... n..... 17.20 17.40 17.60 17.80 5000 m/z 342.00 9.44% 45 91 | 116 146 227 269 315, ) mh—m0n—um“uummnummmmpm] m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsilO)y)t 713 17.20 17.40 17.60 17.80 m/z 325.00 9.21% 147 5000 267 355 429 45 207 i miz-> "40 60 80 100 120140160 180200 220240280280300 320 340 360 380400420/" I * I I « J » J » »J » j > > > t I l > 17.20 17.40 17.60 17.80

LBD.D GCMS1126.M Wed Jan 23 09:02:15 2002 Page 5

NYC-WTC_000018079

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NYC-WTC_000018079Source: NYC Law Department, mirrored locally

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