GCMS blank analysis for sample AD30694, Jan 2002

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Data File C:\HPCHEM\1\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Propanone, 1-(1-methylethoxy Concentration Rank 14

R.T. EstConc Area . Relative to ISTD R.T.

18.16 0.58 ug/1 239973 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Propan e, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 25 2 Butane 58 C4H10 000106-97-8 9 3 2-Bu nol, 2-nitroso-, acetate (est 145 C6H11NO3 013880-90-5 9 4 He.. .ne, 4-ethyl-2,2-dimethyl- 142 C10H22 052896-99-8 9 Abundance Scan 1428 (18.156 min): LBD.D (-) m/z 43.05 100.00% 43

57 73 5000 111 95 17.80 18.00 18.20 18.40 m mmt mrtmpe 85 hmphaT ,201 127 146 m/z 57.00 62.23% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #3286:2-Propanone, 1-(1-methylethoxy)- 43

5000 -P 17.80 18.00 18.20 18.40 27 । 58 73 m/z 73.00 55.66%

m/z-> alsssrm I' ’ ‘ • I TITTpgp 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #62336: Butane 43 T 17.80 18.00 18.20 18.40 7. y— 5000 29 m/z 111.10 42.88% 58 15 1 mtz-> 10 20 30 40 506o7o 80 90 100 110120 130 140 150160170180190 200" Abundance #8596:2-Butanol, 2-nitroso-, acetate (ester) • i • ■ ■ • i ■ ■ ’14,14*14 43 17.80 18.00 18.20 18.40

m/z-> 5000

qr mkmmtm 86 27 56 73 . 115 145 111 < । > k । > । ■ 11111 > 111 ■ < i l p < 1 • 1111 < । < > > 111 > > 111 ■ 111 > 11 ■ । > > 1 ■, > 11 ■ ।

10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 7 17.80 18.00 18.20 18.40 IT

LBD.D GCMS1126.M Wed Jan 23 09:02:20 2002 Page 6

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