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GCMS analysis report, sample AD31502, Feb 2002

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Laboratory report for DEP sample AD31502 documenting analytical results from February 15, 2002.

NYC-WTC_000016593–000016602

Folder label: “GCMS X 12/31/01 A 1/18/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31502.D Vial: 8 Acq On : 18 Jan 2002 10:28 pm Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Misc Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area. Relative to ISTD R.T. --------------------------------------------------------------------- 7.58 0.75 ug/l 193920 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 2-Propanon , 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 2-Propano e, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 3 Ethanol 2,2,2-trichloro- 148 C2H3C13O 000115-20-8 9 4 2-Pent nethiol 104 C5H12S 002084-19-7 5 Abundance Scan 277 (7.584 min): 31502.D (-) m/z 43. 05 100.00

5000

63 72 117 125 7.20 7.40 7.60 7.80 8.00 36 I 0 21, It m/z 46.95 9.22 m/z- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247: 2-Propanone, 1,1,1-trichioro- 43

5000 7.20 7.40 7.60 7.80 8.00 m/z 124.85 8.97 15 35 85 97 117 125 tnlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 bundance 44'3n rC r,, 43

7.20 7.40 7.60 7.80 8.00 5000 m/z 126.90 7.20

15 27 35 63 76 83 93 m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: Ethanol, 2,2,2-trichloro- 1 7.20 7.40 7.60 7.80 8.00 m/z 96.95 6.98 5000 49 77 113 61 150 nlz--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.20 7.40 7.60 7.80 8.00

31502.D GCMS0103.M Wed Feb 06 15:36:44 2002 Page 2

NYC-WTC 000016601

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NYC-WTC_000016601Source: NYC Law Department, mirrored locally

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