GCMS analysis report, sample AD31502, Feb 2002

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Data File : C:\HPCHEM\1\DATA\JAN1802\31502.D Vial: 8 Acq On : 18 Jan 2002 10:28 pm Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 7.45 3.52 ug/l 907417 1,4-Dichlorobenzene-d4 11.50

Tentative ID MW MolForm CAS# Qual Hit# of 5 --------------------------------------------------------------------- 1 3-Pentanol, -methyl- 102 C6H14O 000077-74-7 33 2 Silane, to ramethyl- 88 C4H12Si 000075-76-3 9 3 1-Butana ne, 3-methyl- 87 C5H13N 000107-85-7 7 C3H7NO 000627-45-2 5 4 N-Ethyl ormamide Abundance Scan 262 (7.447 min): 315022.D (-) 73 m/z 72. 100.00 T 5000

3$ I, 50 55 $0 67 ! , 87 103 7.20 7.40 7.60 7.80 m/z 43.05 32.49 miz--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl-

5000 7.20 7.40 7.60 7.80 55 m/z 45.05 12.20 46 s7 27 39 10 20 30----.._40 50 60 70 80 90 100 110 Abundance b45. Sitar e. -• . r ,

73

7.20 7.40 7.60 7.80 5000 m/z 41.00 11.30

45 15 31 55 88 nfz -> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763; 1-Butanamine, 3-methyt- 7.20 7.40 7.60 7.80 m/z 71.00 6.24

5000

i 15 41 55 70 87 10 20 30 40 __- 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31502.D GCMS0103.M Wed Feb 06 15:36:39 2002 Page 1

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