GCMS analysis results for sample AE12327, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12327 conducted on June 4, 2002.

NYC-WTC_000014033–000014053

Folder label: “GCMS X 5/24/02 A 5/28/02”

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NYC 9/11 Public Portal Document ULJLCLY DtaLtll toupOulI KCDOL L

Data File : C:\MSDCHEM\l\DATA\052802\12327.D Vial: 7 Acq On : 28 May 2002 7:11 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Phenanthrene-diO Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.25 ug/L 206984 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# 1 Phenanthrene-diO 188 C14D10 001517-22-2 90 oual 0 2 Anthracene-dlO- 188 C14D10 001719-06-8 87 J • 3 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 3401 (23.062 min): 12327.D (-3396) (-) m/z 188.10 100.00%! 188

5000

80 94 160 22.80 23.00 23.20 23.40

miz-> 0 ■ i. ■ • ■ i' ■" i“ ■ ■ 44 1 ” i” mH 66 J4 1’1110’2771’"T’1E77’I’’ITI 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ■'11 “ I’ ’* m/z 184.10 18.75%| Abundance #79827: Phenanthrene-d10 188

5000 _________ ■ ‘ | __________ . rf r-r ri । i i i , । । । 22.80 23.00 23.20 23.40 80 m/z 94.10 14.92%| 94 160 30 42 52 66 . 11 108118 132 146 , |,| 170179.1,1 0 ‘ 1111111 “' I'111111 “ J11111111 'I nd/t'1 111! > H n . 11. t. .ym. 11IT I ■ > I ■ mtlt’ . r. 11, ■: | flmt .,.. nfe-> 10 2030405060 70 8090 100110120 130140150 160170180190 Abundance #79826: Anthracene-d10- 1(6 - 22.80 23.00 23.20 23.40 5000 m/z 80.05 14.66%

ee 80 94 160 | 17 30 42 52 V J , 108118 132 146 1I 170179] 0 ——————————————————— ■fn-rr n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine ............ ............ ......... , 188 22.80 23.00 23.20 23.40 m/z 189.10 13.93%| 121 5000 173 67 94 39 57 ,| . 84 |, 1JJ 146 133 . .. 161 , II1 0 11 i 11111»»»11:11 111111 (i‘i ।«! 11 j 11 j 11111 j yr rt I it j 1111 t [t ITTNFTtyasanetyeegAaas ........... /z—> 10 2030405060 70 8090 100110120130140150160170180190 22.80 23.00 23.20 23.40

12327.D 052202.M Thu May 30 10:41:12 2002 Page 14

NYC-WTC_000014051

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