GCMS analysis results for sample AE12327, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12327 conducted on June 4, 2002.

NYC-WTC_000014033–000014053

Folder label: “GCMS X 5/24/02 A 5/28/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LIbrary searen compound Report Data File : C:\MSDCHEM\l\DATA\052802\12327.D Vial: 7 Acq On : 28 May 2002 7:11 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 1,5-Naphthalenedithiole Concentration Rank 11 R.T. EstConc• Area Relative to ISTD R.T. 22.54 0.25 ug/L 207393 Phenanthranene- dl 0 22.91 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5/64 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9/59 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-/ 59. Abundance Scan 3312 (22.539 min): 12327.D (-3302) (-) m/z 192.00 100. 00% 1912

5000

40 49 70 82 96 120 146 160 | —A 22.20 22.40 22.60 22.80 T T

O- 11’8 m/z 191.10 18.83% z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole 192

5000 ■ ‘ i ■ ' • ■ i ■ ■

159 22.20 22.40 22.60 22.80 115 128 m/z 193.10 16.10% 40 57 69 79 96 10 147 177 — TPmgTr 0- I’’ nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 1«) 200 Abundance #125856: Phenanthrene, 1-methyl- 192 • ■ i • • ■ • i ■ ■ i ■ ■ ■1 i 1 I 22.20 22.40 22.60 22.80 5000 m/z 146.10 14.47%

27 39 51 63 82 961l 115 126 139 152 190 178 ce 0 ‘ I “ “ I'' " I'' " I' “ ' I ' I ‘ ri 11’11 rI 111117 rrr 11111111 n'| iiii fin > j >‘1‘| 111 rth 1 > i‘ iz-> 2030405060 70 8090 1(X) 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- ■ * | ) L ■ | 19/2 22.20 22.40 22.60 22.80 m/z 82.00 12.00% 5000

n/z—> 29 39 51 63 74 83 * 115 126 139 152 165 176 J, ] 0 ■ i1" ■ i “ " i' “ ■ i ■ ■" i ‘ ■ i ■r' • r11 rr1 ii i [' 11 rn 1111111 2030405060708090 100 110 120 130 140 150 160 170 180190 200 1111 pt 1111 t’t’i 111 rh 111 "’ITT A 22.20 22.40 22.60 22.80

12327.D 052202.M Thu May 30 10:41:12 2002 Page 13

NYC-WTC_000014050

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000014050Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS calculation results for sample AE11602, May 2002 · Box DEP Box 15

NYC-WTC_000013921

GCMS analysis report for sample AE11602 dated June 4, 2002, documenting unknown compounds and surrogate recovery.

1 shared topics · Same agency, volume and box · similarity 0.997