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GCMS analysis results for sample AE11602, June 2002

Machine-extracted title · confidence 90%

TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.

NYC-WTC_000013943–000013967

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document LSC Area Percent Report •Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) *** Title : 209 625/TdLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline -drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 5.677 65 69 81 rBV 80498 173305 5.50% 0.858% 2 8.114 331 335 368 rBV 436557 1154877 36.66% 5.721% 3 8.820 408 412 418 rBV 14428 33348 1.06% 0.165% 4 9.406 472 476 492 rVB 12954 34189 1.09% 0.169% 5 10.313 572 575 577 rW 15902 31951 1.01% 0.158% 6 10.350 577 579 594 rVB 19153 56412 1.79% 0.279% 7 10.524 594 598 602 rBV 20974 45967 1.46% 0.228% 8 12.027 760 762 769 rVB 15274 32605 1.04% 0.162% 9 12.137 769 774 788 rBV 980825 2567095 81.49% 12.716% 10 12.723 832 838 845 rBV 14940 31556 1.00% 0.156% 11 12.980 860 866 870 rBV 43099 117915 3.74% 0.584% 12 13.108 876 880 882 rBV 68366 126541 4.02% 0.627% 13 13.154 882 885 891 rW 131638 258852 8.22% 1.282% 14 13.255 891 896 901 rW 261942 506336 16.07% 2.508% 15 13.346 901 906 909 rW 230014 442738 14.05% 2.193% 16 13.401 909 912 919 rVB 78048 151356 4.80% 0.750% 17 13.511 919 924 933 rBV 283994 548916 17.43% 2.719% 18 14.089 982 987 993 rVB 95610 183474 5.82% 0.909% 19 14.272 1001 1007 1012 rBV 40177 87397 2.77% 0.433% 20 14.354 1012 1016 1021 rVB 48270 94353 3.00% 0.467% 21 15.775 1165 1171 1189 rBV 1544276 3150049 100.00% 15.604% 22 21.081 1744 1750 1761 rBV 1523773 3129565 99.35% 15.503% 23 23.225 1975 1984 1991 rBV 755141 1511424 47.98% 7.487% 24 25.516 2228 2234 2246 rBV2 1244388 2696337 85.60% 13.357% 25 27.495 2445 2450 2459 rVB 28829 55944 1.78% 0.277% 26 33.571 3107 3113 3128 rBV2 757553 1709436 54.27% 8.468% 27 37.786 3565 3573 3592 rBV2 433360 1255322 39.85% 6.218%

Sum of corrected areas: 20187260 11602.D GCMS0520.M Fri May 24 08:33:04 2002

NYC-WTC_0000 13946

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NYC-WTC_000013946Source: NYC Law Department, mirrored locally

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