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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.399 144 148 155 rBV 23084 49105 1.27% 0.225% 2 6.509 155 160 170 rW 39366 101494 2.62% 0.464% 3 6.638 170 174 182 rW 19787 42550 1.10% 0.195% 4 6.748 182 186 193 rW 27217 55666 1.44% 0.255% 5 7.776 294 298 310 rBV 66412 162844 4.20% 0.745%

6 10.439 583 588 596 rBV 20510 41512 1.07% 0.190% 7 11.513 701 705 rBV2 715 13653 38889 1.00% 0.178% 8 11.641 715 719 727 rW 31093 69364 1.79% 0.317% 9 11.788 727 735 747 rW 1078295 2692964 69.54% 12.316% 10 15.396 1121 1128 1145 rBV 1651278 3737483 96.51% 17.093%

11 20.684 1696 1704 1718 rBV 1724484 3872634 100.00% 17.711% 12 25.118 2179 2187 2198 rBV 1626971 3528878 91.12% 16.139% 13 27.110 2399 2404 2410 rBV 51824 96159 2.48% 0.440% 14 29.534 2662 2668 2676 rBV2 113486 218760 5.65% 1.000% 15 29.653 2676 2681 2687 rW 28351 55285 1.43% 0.253%

16 30.727 2792 2798 2806 rBV 42943 89561 2.31% 0.410% 17 31.673 2893 2901 2906 rBV2 89039 172791 4.46% 0.790% 18 31.764 2906 2911 2918 rW 88424 180196 4.65% 0.824% 19 32.765 3014 3020 3028 rBV 87376 185002 4.78% 0.846% 20 33.160 3055 3063 3073 rBV2 1316012 3067650 79.21% 14.030% 21 33.720 3114 3124 3131 rBV2 106222 238402 6.16% 1.090% 22 34.638 3220 3224 3233 rVB 79734 168479 4.35% 0.771% 23 35.528 3317 3321 3327 rBV 67160 145989 3.77% 0.668% 24 36.391 3411 3415 3424 rBV 39900 100528 2.60% 0.460% 25 37.273 3503 3511 3527 rBV2 932685 2753167 71.09% 12.591%

Sum of corrected areas: 21865352 22546.D NP091101.M Wed Oct 03 14:44:18 2001

NYC-WTC_000086955

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