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GC/MS analysis results for sample AD22582, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.384 141 146 152 rBV 26124 53564 1.50% 0.269% 2 6.494 154 158 162 rBV 38504 82023 2.30% 0.412% 3 6.631 169 173 179 rVB 18917 38620 1.08% 0.194% 4 6.742 181 185 192 rVB 28198 55422 1.55% 0.278% 5 11.644 713 719 729 rBV 29467 70536 1.98% 0.354%

6 729 735 753 rBV 999333 2529919 70.86% 12.707% 7 1122 1128 1144 rBV 1547735 3483189 97.56% 17.495% 8 2Tr7'686- 1697 1704 1719 rBV 1604417 3570238 100.00% 17.932% 9 25.121 2180 2187 2200 rBV2 1539286 3267136 91.51% 16.409% 10 29.545 2663 2669 2674 rBV 135360 268733 7.53% 1.350% 11 29.656 2677 2681 2686 rVB 26901 53528 1.50% 0.269% 12 29.784 2691 2695 2703 rVB 19392 39557 1.11% 0.199% 13 30.739 2794 2799 2804 rVB 40886 82051 2.30% 0.412% 14 31.675 2896 2901 2907 rBV 106704 208581 5.84% 1.048% 15 31.767 2907 2911 2917 rW 76479 162025 4.54% 0.814% 16 32.768 3013 3020 -3027 rBV 82989 174249 4.88% 0.875% 17 ■33.16» 3056 3063 3076 rBV2 1163038 2752481 77.10% 13.824% 18 33.722 3113 3124 3130 rBV 97255 215720 6.04% 1.083% 19 34.641 3220 3224 3234 rVB 71822 147673 4.14% 0.742% 20 35.531 3316 3321 3326 rBV 63927 138906 3.89% 0.698% 21 36.403 34n~3416 3421 rBV 38985 89450 2.51% 0.449% 22 3-7-^84 3504 3512 3524 rBV2 842515 2426587 67.97% 12.188%

Sum of corrected areas: 19910188 22582.D NP091101.M Wed Oct 03 12:08:52 2001

NYC-WTC_000087256

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NYC-WTC_000087256Source: NYC Law Department, mirrored locally

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