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GC/MS analysis results for sample AD22579, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087180–000087201

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File ; C:\HPCHEM\l\DATA\SEP2801\22579.D Vial: 7 Acq On : 28 Sep 2001 6:18 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total / 1 6.397 144 148 154 rBV 31484 66133 1.61% 0.293% 2 6.507 155 160 171 rW 48546 128964 3.15% 0.572% 3 6.635 171 174 180 rW 27219 56494 1.38% 0.250% 4 6.755 182 187 194 rW 38403 77032 1.88% 0.341% 5 11.648 715 720 729 rVB 33725 79039 1.93% 0.350% 6 729 735 750 rBV 1227054 2835775 69.20% 12.569% 7 1122 1129 1142 rBV 1777384 3927056 95.84% 17.406% 8 2«-r690 1697 1705 1720 rBV 1868461 4097717 100.00% 18.163% 9 2180 2188 2199 rBV2 1749254 3856878 94.12% 17.095% 10 29.540/ 2664 2669 2673 rBV 84925 155434 3.79% 0.689% 11 29.650 2677 2681 2687 rVB2 32388 48684 1.19% 0.216% 12 30.734 2795 2799 2804 rVB 29460 58312 1.42% 0.258% 13 31.679J 2897 2902 2907 rBV2 78872 160126 3.91% 0.710% . 14 31.771'J 2907 2912 2919 rW 53711 105403 2.57% 0.467% 15 32.762J 3016 3020 3027 rVB 53610 105592 2.58% 0.468% 16 3056 3064 -3074 rBV2 1443427 3314142 80.88% 14.690% 17 33.717 3117 3124 3132 rVB2 64881 150482 3.67% 0.667% 18 34.644,/ 3221 3225 3232 rVB 55372 111210 2.71% 0.493% 19 35.535d 3318 3322 3327 rBV 47371 100042 2.44% 0.443% 20 36.398^ 3412 3416 3420 rVB 32660 66903 1.63% 0.297% 21 e-T-r-S-aa. 35Ot~-3513 3533 rVB2 1025055 3059733 74.67% 13 .3'52^

Sum of corrected areas: 22561151 22579.D NP091101.M Tue Oct 02 11:49:56 2001

NYC-WTC_000087185

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NYC-WTC_000087185Source: NYC Law Department, mirrored locally

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