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GC/MS analysis results for sample AD22580, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22580 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087202–000087225

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\SEP2801\22580.D Vial: 8 Acq On : 28 Sep 2001 7:17 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling s 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 6.402 *^ 144

0 148 155 rBV 46839 88213 2.06% 0.363% 6.503^ 155 159 163 rBV 66844 132061 3.09% 0.544% 6.640 y 170 174 182 rVB 35687 65243 1.52% 0.269% 6.751< 182 186 194 rBV 47081 91579 2.14% 0.377% 11.644 J 714 719 728 rBV 35707 82561 1.93% 0.340% 6 728 734 752 rBV 1259384 2928488 68.43% 12.066% 7 ^57-3-9^ 1121 1128 1144 rBV 1694788 4067951 95.05% 16.761% 8 ^20-. 686- 1695 1704 1722 rBV 1760164 4279761 100.00% 17.634% 9 aS-viZXUi 2178 2187 2198 rBV2 1770889 3965410 92.65% 16.338% 10 29.536 J 2663 2668 2674 rBV 107150 220946 5.16% 0.910% 11 29.655 , 2677 2681 2686 rW 30567 57452 1.34% 0.237% 12 30.739Y 2794 2799 2805 rVB 46056 94737 2.21% 0.390% 13 31.675' 2895 2901 2906 rBV 89955 173899 4.06% 0.717% 14 31.767 J/2906 2911 2916 rBV 86681 179724 4.20% 0.741% 15 32.768’' 3015 3020 3025 rBV 95404 190957 4.46% 0.787% 16 ■3J.162 ( 3056 3063 '3075 rBV2 1439700 3570605 83.43% 14.712% 17 33.722 3117 3124 3129 rVB2 113559 234857 5.49% 0.968% 18 34.640 3213 3224 3234 rBV 88100 222813 5.21% 0.918% 19 35.531 3317 3321 3329 rVB 82724 172124 4.02% 0.709% 20 36.394 3411 3415 3420 rVB 53565 117391 2.74% 0.484% 21 T7-72^ 35(r?r3513 3528 rVB2 1067136 3282214 76.69% 13.524% 22 38.413 3631 3635 3640 rVB3 18965 51360 1.20% 0.212%

Sum of corrected areas: 24270346 22580.D NP091101.M Wed Oct 03 11:37:29 2001

NYC-WTC_000087207

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