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GCMS analysis results for sample AE06455, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039588–000039610

Folder label: “GCMS X 3/19/02 A 4/17/02

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Scanned page image, NYC-WTC_000039593
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\APR17O2\6455. D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.100 329 333 346 rBV 100779 258750 8.00% 1.531% 2 8.247 346 349 362 rVB 16452 46716 1.45% 0.276% 3 11.616 712 716 724 rBV 19146 44269 1.37% 0.262% 4 12.213 775 781 797 rVB 940774 2313403 71.56% 13.689% 5 14.811 1059 1064 1070 rBV 103246 195478 6.05% 1.157%

6 15.848 1170 1177 1192 rBV 1382964 2924628 90.47% 17.305% 7 17.969 1402 1408 1414 rVB 142945 266335 8.24% 1.576% 8 18.685 1481 1486 1491 rBV 63761 117263 3.63% 0.694% 9 20.796 1710 1716 1723 rBV 99730 202526 6.26% 1.198% 10 21.145 1748 1754 1766 rBV 1610924 3232773 100.00% 19.129%

11 21.558 1792 1799 1808 rVB 36564 72115 2.23% 0.427% 12 23.321 1986 1991 1996 rVB 95102 175488 5.43% 1.038% 13 25.497 2222 2228 2232 rBV 72231 140480 4.35% 0.831% 14 25.588 2232 2238 2249 rW 1403904 2944723 91.09% 17.424% 15 27.424 2432 2438 2444 rVB 48286 92170 2.85% 0.545%

16 29.187 2625 2630 2636 rVB 35439 71690 2.22% 0.424% 17 30.656 2785 2790 2797 rVB 183587 362075 11.20% 2.142% 18 30.784 2797 2804 2810 rBV 31782 65157 2.02% 0.386% 19 32.244 2955 2963 2968 rBV2 26300 57084 1.77% 0.338% 20 33.639 3107 3115 3128 rBV2 825110 1869666 57.83% 11.063%

21 33.860 3134 3139 3145 rVB 26907 53163 1.64% 0.315% 22 34.897 3247 3252 3259 rBV2 17257 39456 1.22% 0.233% 23 37.872 3567 3576 3591 rBV2 457704 1354722 41.91% 8.016%

Sum of corrected areas: 16900130

6455.D GCMS0412.M Thu Apr 18 09:14:10 2002

NYC-WTC_000039593

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NYC-WTC_000039593Source: NYC Law Department, mirrored locally

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