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GCMS analysis results for sample AE06635, April 2002

Machine-extracted title · confidence 100%

DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.

NYC-WTC_000060478–000060494

Folder label: “GCMS X 3/21/02 A 4/16/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APR16 02\6635.D Vial : 8 Acq On 16 Apr 2002 8:03 pm Operator: Sample gc/ms scan 3/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C;\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.Ti first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.208 772 780 797 rBV 1161418 2876628 68.10% 12.264% 2 14.815 1058 1064 1069 rVB 167785 330642 7.83% 1.410% 3 15.844 1170 1176 1193 rBV 1821411 3672741 86.95% 15.659% 4 21.150 1747 1754 1769 rBV 2072827 4223850 100.00% 18.008% 5 25.584 2231 2237 2246 rBV2 1854164 4037067 95.58% 17.212%

6 30.661 2785 2790 2796 rBV 223030 426518 10.10% 1.818% 7 33.277 3069 3075 3090 rBV 143571 338271 8.01% 1.442% 8 33.644 3107 3115 3134 rBV2 1336179 3050514 72.22% 13.006% 9 33.865 3134 3139 3149 rVB 67224 169833 4.02% 0.724% 10 34.902 3245 3252 3259 rBV3 28569 85466 2.02% 0.364%

11 36.095 3375 3382 3395 rBV2 68525 248058 5.87% - 1.058% 12 37.316 3507 3515 3544 rBV2 90540 439537 10.41% 1.874% 13 37.876 3567 3576 3588 rBV2 800609 2428242 57.49% 10.353% 14 38.749 3663 3671 3696 rBV3 82089 456391 10.81% 1.946% 15 40.502 3848 3862 3878 rBV2 55349 350725 8.30% 1.495%

16 42.669 4085 4098 4112 rBV4 30397 213473 5.05% 0.910% 17 45.386 4383 4394 4407 rBV6 14043 107197 2.54% 0.457%

Sum of corrected areas: 23455153

6635.D GCMS0412.M Wed Apr 17 12:03:01 2002

NYC-WTC_000060483

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NYC-WTC_000060483Source: NYC Law Department, mirrored locally

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