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GCMS analysis results for sample AE04035, Mar 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE04035 dated March 29, 2002.

NYC-WTC_000038580–000038593

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4035.D Vial: 41 *Acq On : 24 Mar 2002 9:33 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.267 781 787 805 rVB 936532 2288742 63.96% 12.511% 2 14.865 1064 1070 1075 rVB 120893 236936 6.62% 1.295% 3 15.902 1177 1183 1198 rBV 1545878 3150435 88.05% 17.221% 4 21.209 1755 1761 1779 rBV 1746875 3578208 100.00% 19.560% 5 25.652 2239 2245 2256 rBV2 1585079 3519947 98.37% 19.241%

6 27.626 2454 2460 2467 rBV 20829 40499 1.13% 0.221% 7 30.729 2793 2798 2807 rBV 215075 411404 11.50% 2.249% 8 33.721 3117 3124 3142 rBV2 1131886 2610029 72.94% 14.267% 9 33.933 3142 3147 3155 rVB 79607 177076 4.95% 0.968% 10 36.154 3384 3389 3396 rBV 14312 39098 1.09% 0.214%.

11 37.393 3518 3524 3537 rBV 26430 94277 2.63% 0.515% 12 37.972 3578 3587 3604 rBV 607215 1825756 51.02% 9.980% 13 38.853 3675 .3683 3694 rBV2 29145 129004 3.61% 0.705% 14 40.616 3867 3875 3889 rBV4 20024 106667 2.98% 0.583% 15 42.828 4104 4116 4133 rBV6 13239 85599 2.39% 0.468%

Sum of corrected areas: 18293677

4035.D GCMS0308.M Tue Mar 26 10:48:00 2002

NYC-WTC_000038585

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NYC-WTC_000038585Source: NYC Law Department, mirrored locally

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