GCMS chromatogram data for sample AE04592, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR2602\4592.D Vial: 8 Acq On : 26 Mar 2002 4:38 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100. Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total.

1 8.133 332 336 349 rBV 98108 243177 5.53% 1.047% 2 12.255 779 785 803 rVB 1214736 2999818 68.27% 12.916% 3 15.890 1174 1181 1198 rBV 1914890 3985507 90.71% 17.161% 4 21.197 1752 1759 1777 rBV 2094816 4393878 100.00% 18.919% 5 25.640 2236 2243 2254 rBV 1934483 4164882 94.79% . 17.933%

6 30.707 2790 2795 2802 rBV 212026 422016 9.60% 1.817% 7 33.700 3112 3121 3132 rBV2 1063862 2569111 58.47% 11.062% 8 34.949 3250 3257 3272 rBV 93491 260547 5.93% 1.122% 9 36.142 3380 3387 3409 rBV 170156 546770 12.44% 2.354% 10 37.372 3513 3521 3546 rBV 165876 693637 15.79% 2.987%

11 37.942 3573 3583 3600 rBV2 555028 1656776 37.71% 7.134% 12 38.832 3669 3680 3706 rBV2 117073 624929 14.22% 2.691% 13 40.595 3861 3872 3892 rBV2 63601 386122 8.79% 1.663% 14 42.789 4097 4111 4128 rBV4 31607 209515 4.77% 0.902% 15 45.534 4401 4410 4423 rVB5 10648 68160 1.55% 0.293%

Sum of corrected areas: 23224845

4592.D GCMS0308.M Thu Mar 28 16:27:37 2002

NYC-WTC_000058396