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GCMS analysis results for sample AE01462, Feb 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.

NYC-WTC_000038642–000038656

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

‘ Data File : C:\HPCHEM\1\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.359 140 143 152 rVB 15942 34301 1.32% 0.219% 2 7.727 287 292 298 rBV 22823 47001 1.81% 0.300% 3 8.222 340 346 353 rBV2 40062 109194 4.20% 0.698% 4 12.326 788 793 803 rBV 760005 1858604 71.41% 11.875% 5 15.971 1184 1190 1202 rBV 1181356 2434009 93.52% 15.551%

6 21.286 1763 1769 1785 rBV 1265227 2602728 100.00% 16.629% 7 22.590 1907 1911 1917 rBV 22058 40837 1.57% 0.261% 8 24.031 2057 2068 2072 rBV 66531 129090 4.96% 0.825% 9 24.104 2072 2076 2083 rVB2 13492 30369 1.17% 0.194% 10 25.390 2209 2216 2220 rBV2 34593 70656 2.71% 0.451%

11 25.738 2247 2254 2264 rBV2 1147112 2484756 95.47% 15.875% 12 28.979 2602 2607 2615 rBV 29023 73304 2.82% 0.468% 13 30.806 2801 2806 2812 rBV 151418 318133 12.22% 2.033% 14 31.311 2856 2861 2877 rBV 722297 1566994 60.21% 10.011% 15 33.808 3126 3133 3143 rBV 877919 2055858 78.99% 13.135%

L6 38.086 3590 3599 3621 rBV2 553558 1796210 69.01% 11.476%

Sum of corrected areas: 15652044

1462.D GCMS0308.M Mon Mar 25 08:27:02 2002

NYC-WTC_000038645

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