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GCMS analysis results for sample AE01503, Mar 2002

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Laboratory report documenting GCMS analysis of sample AE01503 conducted on March 6, 2002.

NYC-WTC_000003591–000003606

Folder label: “GCMS X 1/23/02 A 2/22/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File : C:\HPCHEM\1\DATA\FEB2102\1503.D Vial: 26 Acq On : 22 Feb 2002 4:46 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.032 758 761 771 rVB 7954 20524 1.10% 0.203% 2 12.261 782 786 789 rBV 13612 31342 1.68% 0.310% 3 12.335 789 794 807 rVB 578644 1378968 74.07% 13.623% 4 15.970 1184 1190 1203 rBV 829788 1764756 94.79% 17.435% 5 21.285 1763 1769 1783 rBV 934820 1861699 100.00% 18.392%

6 24.030 2064 2068 2073 rVB 21040 36974 1.99% 0.365% 7 25.380 2210 2215 2220 rVB2 15110 31451 1.69% 0.311% 8 25.738 2247 2254 2261 rBV2 814512 1774964 95.34% 17.536% 9 27.693 2462 2467 2471 rBV 17159 33534 1.80% 0.331% 10 28.979 2602 2607 2611 rBV 40283 84852 4.56% 0.838%

11 29.089 2616 2619 2625 rW3 7448 20100 1.08% 0.199% 12 30.805 2802 2806 2812 rVB 112694 231313 12.42% 2.285% 13 31.310 2855 2861 2873 rBV 111042 253680 13.63% 2.506% 14 33.798 3126 3132 3145 rBV2 565022 1337959 71.87% 13.218% 15 34.009 3151 3155 3163 rVB2 8568 22408 1.20% 0.221%

16 36.277 3396 3402 3424 rBV 53774 208726 11.21% 2.062% 17 38.076 3589 3598 3613 rBV2 324001 1028829 55.26% 10.164%

Sum of corrected areas: 10122079

1503.D GCMS0208.M Tue Feb 26 15:12:21 2002

NYC-WTC_000003596

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NYC-WTC_000003596Source: NYC Law Department, mirrored locally

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