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GCMS analysis results, sample AE05234, April 2002

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Laboratory report documenting GCMS analysis of sample AE05234 for unknown compounds on April 9, 2002.

NYC-WTC_000059156–000059171

Folder label: “GCMS X 3/9/02 A 3/30/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\MAR3OO2\5234.D Vial: 45 Acq On : 31 Mar 2002 12:37 pm Operator: Sample : gc/ms scan 3/9 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.142 332 337 344 rBV 25560 63755 1.75% 0.367% 2 8.721 397 400 413 rBV 37370 129260 3.55% 0.745% 3 10.401 575 583 594 rVB 26993 93602 2.57% 0.539% 4 12.246 779 784 799 rBV 1040491 2472541 67.97% 14.250% 5 14.844 1062 1067 1073 rVB 19784 38376 1.06% 0.221%

6 15.881 1174 1180 1197 rBV 1540759 3195114 87.84% 18.415% 7 21.188 1752 1758 1770 rBV 1745901 3637435 100.00% 20.964% 8 25.631 2235 2242 2253 rBV2 1574580 3359183 92.35% 19.360% 9 27.366 2426 2431 2440 rBV2 25577 61891 1.70% 0.357% 10 30.707 2789 2795 2802 rBV 243891 490174 13.48% 2.825%

11 33.691 3113 3120 3134 rBV2 832486 1903880 52.34% 10.973% 12 33.911 3139 3144 3155 rVB 39895 98319 2.70% 0.567% 13 37.932 3574 3582 3600 rBV2 420677 . 1272540 34.98% 7.334% 14 39.888 3784 3795 3810 rBV3 61367 266149 7.32% 1.534% 15 40.521 3850 3864 3871 rBV7 49464 228812 6.29% 1.319%

16 43.138 4139 4149 4162 rVBlO 7794 39908 1.10% 0.230%

Sum of corrected areas: 17350939

5234.D GCMS0308.M Wed Apr 03 13:58:57 2002

NYC-WTC_000059161

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NYC-WTC_000059161Source: NYC Law Department, mirrored locally

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