GCMS analysis results for sample AE04411, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\MAR2502\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.253 779 785 800 rVB 1066166 2547995 68.70% 8.783% 2 14.851 1063 1068 1072 rBV2 45170 89404 2.41% 0.308% 3 15.888 1175 1181 1197 rBV 1624173 3368718 90.82% 11.612% 4 21.194 1752 1759 1770 rBV 1775150 3709133 100.00% 12.786% 5 25.638 2236 2243 2254 rBV 1666069 3488751 94.06% 12.026%

6 30.705 2790 2795 2804 rBV 228665 464852 12.53% 1.602% 7 33.698 3112 3121 3138 rBV2 945486 2190471 59.06% 7.551% 8 34.946 3250 3257 3271 rBV2 39873 117291 3.16% 0.404% 9 36.140 3381 3387 3407 rBV2 233170 794313 21.42% 2.738% 10 37.379 3513 3522 3549 rBV 455709 1978386 53.34% 6.820% 11 37.939 3574 3583 3601 rBV 523172 1514753 40.84% 5.222% 12 38.830 3670 3680 3724 rBV2 497301 2870666 77.39% 9.896% 13 40.601 3859 3873 3917 rBV2 371944 2797533 75.42% 9.643% 14 42.796 4095 4112 4144 rBV2 218644 1952899 52.65% 6.732% 15 45.550 4392 4412 4436 rBV3 115722 1124455 30.32% 3.876%

Sum of corrected areas: 29009620

4411.D GCMS0308.M Thu Mar 28 12:33:24 2002

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